نتایج جستجو برای: electrospray ionization esi
تعداد نتایج: 47193 فیلتر نتایج به سال:
Development of nanoinjector devices for electrospray ionization - tandem mass spectrometry (ESI-MSn)
We used multilocus PCR and electrospray ionization mass spectrometry (PCR/ESI-MS) to determine the genotype and drug resistance profiles for 96 Mycobacterium tuberculosis isolates circulating in regions of high and low tuberculosis (TB) endemicity in China. The dominant principal genetic group (PGG) circulating in China was PGG1, and drug-resistant gene mutations were more diversified in the re...
We present the first use of digital microfluidic techniques to perform on-chip solid phase extraction (SPE). The material used for SPE was a porous polymer monolith with 12-carbon functionality (C12 PPM) which was photopolymerized on-chip and used to desalt a peptide sample prior to nano-electrospray ionization mass spectrometric analysis (nano-ESI-MS). We anticipate this technique may be usefu...
A technique for the continuous on-line monitoring of polymerization processes by electrospray ionization mass spectrometry (ESI-MS) is presented via coupling with a commercial microreactor system. The potential is demonstrated by monitoring polymerizations in real time under synthesis conditions. Furthermore, a single acrylate monomer insertion into a oligo-RAFT agent, as used in the synthesis ...
Electrospray ionization/tandem mass spectrometry of proteins separated on sodium dodecylsulfate polyacrylamide gel electrophoresis (SDS-PAGE) gels is severely limited by the requirement that the protein be completely separated from the SDS. As shown here, the gaseous noncovalent SDS adducts of protonated proteins thus formed can be dissociated by infrared irradiation. ESI spectra from myoglobin...
A novel strategy was developed to extend the application of electrospray ionization (ESI) Fourier transform ion cyclotron resonance (FTICR) mass spectrometry (MS) to the analysis of long-chain polysaccharides. High molecular weight polydisperse maltodextrins (poly-alpha(1-4) glucose) and dextrans (poly-alpha(1-6) glucose) were chosen as model compounds in the present study. Increased ionization...
Abstract Ultra high-resolution mass spectrometry (FT-ICR MS) coupled to electrospray ionization (ESI) provides unprecedented molecular characterization of complex matrices such as petroleum products. However, ESI faces major competition phenomena that prevent the absolute quantification compounds interest. On other hand, comprehensive two-dimensional gas chromatography (GC × GC) specific detect...
Fast and efficient handling of ligands biological targets are required in bioaffinity screening based on native electrospray ionization mass spectrometry (ESI-MS). We use a prototype microfluidic autosampler, called the “gap sampler”, to sequentially mix individual small molecule together with target protein compare results data from thermal shift assay surface plasmon resonance. In first round...
a quantitative analysis method for fudosteine in human serum by high-performance liquid chromatography-electrospray ionization tandem mass spectrometry (hplc-esi/ms/ms) was established, which shows high sensitivity and selectivity. the mobile phase composition was 75% 20 mm acetic acid and 25% acetonitril, which was pumped at a flow rate of 0.40 ml/min. the overall chromatographic run time was ...
the occurrence of emerging fusarium mycotoxins beauvericin (bea), enniatins (enns) (a, a1, b, b1), fusaproliferin and moniliformin was evaluated by a liquid chromatography/electrospray ionization-tandem mass spectrometric (lc/esi-ms/ms) technique in 65 domestic rice samples produced in gilan and mazandaran provinces in ir iran. the results showed that 46% of the samples were contaminated with a...
نمودار تعداد نتایج جستجو در هر سال
با کلیک روی نمودار نتایج را به سال انتشار فیلتر کنید