نتایج جستجو برای: fast and green synthesis
تعداد نتایج: 16952763 فیلتر نتایج به سال:
the synthesis of nb doped batio3 has been investigated under microwave-hydrothermal (mh) conditions in the temperature of 150°c for only 2 h using c16h36o4ti, bah2o2.8h2o and nbcl5 as ba, ti and nb sources, respectively. typical experiments performed on mh processing have not yet reported for nb doped batio3. in the mh process, the formation of high purity nano tetragonal nb-batio3 was stron...
A simple, mild and high efficient procedure for one pot three component synthesis of 2-amino 4-H chromene derivatives was studied. The reaction was performed in water using aryl aldehydes, malononitrile and resorcinol, phloroglucinol or naphthole in the presence of N-methyl D-glucamine (Meglumine) as a green high efficient catalyst. The reaction was studied in thermal, microwave (MW) and ultras...
An environmentally friendly, green, and highly efficient process for the synthesis of biologically and pharmacologically 4H-benzo[b]pyrans and 3,4-dihydropyrano [c] chromenes is developed by condensing cyclic aromatic aldehydes, malononitrile, and dimedone or 4‐hydroxycoumarin in the presence of lactic acid as an efficient and green catalyst. The corresponding products have b...
In this study an easy, green, efficient and simple approach is reported for the synthesis of some benzothiazole-, benzimidazole- and benzoxazole-2-thiolderivatives. The proposed approach employs the reaction of corresponding aromatic amine with potassium isopropyl xanthate (Z11) in the presence of copper sulfate (CuSO4) as a catalyst under conventional heating and ultrasonic irr...
abstract: advertisements are the most accessible type of authentic materials, and this is one reason why they are used more and more in english teaching classes. for this cause, studies in the field of advertisements are very widespread nowadays. for pun is one aspect which makes advertisements more interesting, it is used more than before in advertisements. use of puns makes an advertisement m...
a simple, mild and high efficient procedure for one pot three component synthesis of 2-amino 4-h chromene derivatives was studied. the reaction was performed in water using aryl aldehydes, malononitrile and resorcinol, phloroglucinol or naphthole in the presence of n-methyl d-glucamine (meglumine) as a green high efficient catalyst. the reaction was studied in thermal, microwave (mw) and ultras...
Nano sulfated titania was tested as solid acid heterogeneous catalyst for the synthesis of 4-(Trifluoromethyl) coumarin and coumarin derivatives under solvent-free condition. Factorial design evidenced a positive effect of reaction temperature, amount of catalyst, and solvents. This nano-sized sulfated titania has been prepared by a sol-gel hydrothermal process. The prepared sulfated titania s...
An effective one-pot synthesis of dihydropyrimidinonoes in solvent free conditions using CuCl2 as an inexpensive and readily available reagent through Biginelli condensation reaction of aldehyde derivatives, 1,3-dicarbonyl compounds and urea is described. Excellent yields, short reaction times for formation of the products and simple work-up are attractive features of this green protocol.
An efficient and environmentally benign procedure for synthesis of triarylmethanes is developed via condensation of aromatic aldehydes and N,N-dimethylaniline using small quantity of heteropolyphosphotungstic acid (HPW) as catalyst in water. Good functional group tolerance, simple green experimental procedure, and good to excellent yields of products are the most advantages of this work.
In this study, a one-pot and efficient method is reported for the synthesis of symmetrical disulfides from alkyl halides in the present of sulfur and 1-butyl-3-methylimidazolium hydroxide as a basic reagent and phase transfer catalyst. The reaction proceeded very fast and afforded the desired products in moderate to excellent isolated yields.
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