A method of microwave-assisted extraction coupled with high-speed counter-current chromatography was established for separation and purification of isopimpinellin, pimpinellin and phellopterin from Toddalia asiatica (L.) Lam. The conditions of MAE including the extraction solvent, size of sample, solid/liquid ratio, extraction temperature and extraction time were optimized by a mono-factor test...

The use of microwave heating for preparation in organic synthesis has been accepted as an effective technique in synthesis due to the significant advantages over the conventional method. In the present work, microwave heating was applied to the preparation of atrazine (template molecule) magnetic molecularly imprinted polymer (mag-MIP) beads by suspension polymerization. The term of the polymer...

chaetomorpha sp is one of the persian gulf green algae which can be a marine source of natural antioxidants such as polyphenols. industrial and economic development of these materials is influenced by effective extraction and application methods. microwave-assisted extraction (mae) and ultrasound-assisted extraction (uae) are novel techniques which have a potential to apply in laboratory with a...

2. Soxhlation: Soxhlet extraction is only required where the desired compound has a limited solubility in the solvent, and the impurity is insoluble in that solvent. If the desired compound has a high solubility in a solvent then a simple filtration can be used to separate the compound from the insoluble substance [1]. In a conventional soxhlet system plant material is placed in thimble-holder,...

Pectin was extracted from lime flavedo, albedo and pulp by employing microwave-assisted extraction (MAE) under pressure. Heating times ranged from 1 to 10min. Optimal time of heating was 3min. Molar mass, viscosity, radius of gyration and hydrated radius were found to decrease with heating time. At 3min heating time, depending on the lime fraction which was extracted, weight average molar mass ...