The effects of FC-4 cationic surfactant on electrodeposited Ag–PTFE composite coating using direct or pulsed currents were studied using scanning electron microscope (SEM), energy dispersive X-ray (EDS), optical microscope, and a linear tribometer. FC-4:PTFE in various ratios were added to a non-cyanide succinimide silver complex bath. Direct or pulsed current method was used at a constant curr...

The as-grown structure of electrochemically synthesized titania nanotube arrays is investigated by scanning electron microscope (SEM) in combination with transmission electron microscope (TEM) as well as X-ray diffraction (XRD). The analysis reveals a preferred growth direction of the nanotubes relative to the substrate surface and the well control on the nanotube arrays morphology. The crystal...

To investigate transition metal precipitates in Si, synchrotron based measurements, like micro x-ray fluorescence (μXRF) or detailed transmission electron microscopy (TEM) studies, are usually necessary. Transition metals are among the most detrimental defects in multi-crystalline (mc) silicon material for solar cell applications, due to their impact on minority charge carrier lifetime and poss...

The Sintering behavior and kinetic evaluation of the bio-ceramics from bovine bone are investigated by stepwise isothermal dilatometry (SID), X-ray diffraction (XRD) and scanning electron microscope (SEM). The isothermal shrinkage data obtained from SID could be well analyzed to get kinetic parameters according to the empirical rate equation developed by Makipirtti-Meng, dY/dt = nk(T)Y(1-Y)[Y/(...

Nanoparticles of titanium dioxide doped with Fe2+ ions have been synthesized via sol-gel technique using Titanium tetraisopropoxide (TTIP) and ferrous sulphate as a precursors. The synthesized nanopowders were characterized by Powder X-ray Diffraction (PXRD), Scanning Electron Microscope (SEM), Fourier Transform Infrared (FTIR), Ultraviolet Visible (UV-Vis) and Photoluminescence (PL) Spectrosco...

Cadmium Sulfide crystals were grown by direct vapor transport (DVT) from high-purity starting materials. The grown CdS crystals were orange in color, transparent, dendrite platelets shaped were observed. The structure of CdS crystals has been studied with the help of X-ray diffraction (XRD) and Transmission Electron Microscope (TEM). The crystals grown by DVT technique possess hexagonal structu...

Copper-based chalcogenides that contain abundant, low-cost and environmentally-friendly elements, are excellent materials for numerous energy conversion applications, such as photocatalysis, photovoltaics, photoelectricity and thermoelectrics (TE). Here, we present a high-yield and upscalable colloidal synthesis route for the production of monodisperse ternary I-III-VI₂ chalcogenides nanocrysta...

a simple and facile method for the preparation offe2+ supported on hydroxyapatite-core-shell-γ-fe2o3 nanoparticles (γ-fe2o3@hap-fe2+ nps) as an environmentally friendly and recyclable green catalyst is described and used for the one-pot synthesis of benzimidazoles and benzoxazole derivatives via reactions between aromatic aldehydes and ortho‐phenylenediamine or ortho‐aminophenol in aqueous medi...

the mechanical properties and microstructural developments of 321 stainless steel during thermomechanicalprocess were investigated. the repetitive cold rolling and subsequent annealing wereconducted to achieve nanocrystalline structure in an aisi 321 stainless steel. heavily cold rolling at−20°c was conducted to form martensite in metastable austenitic steel. the process was followed byannealin...

A new planktonic species of the marine water mites family Pontarachnidae Koenike, 1910 is described from Corozal Bay, an estuarine system in Belize. The morphological description includes Scanning Electronic Microscope (SEM) images and augmented by analysis DNA cytochrome c oxidase I (COI) sequences, barcode, used for first time a this group.