In the current study, the recrystallization behavior of 75% cold-rolled Fe-22Mn-10Al-1.4C steel during annealing at 750, 770, 790, 810, and 830°C was studied. X-ray diffraction patterns and optical microscopy were used to characterize microstructures. The Vickers Micro-hardness test was used to characterize recrystallization kinetics during annealing. Johnson-Mehl-Avrami-Kolmogorov (JMAK) model...

Synchrotron Radiation (SR) based techniques such as SR-μ Fourier Transform InfraRed (FTIR) spectroscopy, SR-μ X-Ray Fluorescence (XRF), SR-μ X-Ray Absorption Near Edge Spectroscopy (XANES) and SR-μ X-Ray Diffraction (XRD) are increasingly used for the study of cultural heritage materials, as they offer enhanced spatial resolution and chemical sensitivity. For such analyses, painting fragments a...

catalytically graphitized electrospun carbon nanofibers adorned uniformly with fine nickel nanoparticles were successfully prepared. the procedure was based on the electrospinning technique and the use of nickel precursor to create both graphitized nanofibers and nickel nanoparticles under a relatively low-temperature heat treatment. the x-ray diffraction and raman results clearly proved cataly...

Nanostructured ZnO thin films have been deposited using a successive chemical solution deposi method. The structural, morphological, electrical and sensing properties of the films were studied different concentrations of Al-dopant and were analyzed as a function of rapid photothermal proces temperatures. The films were investigated by X-ray diffraction, scanning electron microscopy, en dispersi...

Metal matrix composite coatings reinforced with nano-particles have attracted scientific and technological interest due to the enhanced properties exhibited by these coatings. Cobalt/hexagonal boron nitride nano-composite coatings were prepared by means of the pulse current electroplating from a chloride electrolyte on copper substrates and a comparison was made with the pure cobalt in terms of...

Due to their aesthetic value and high compressive strength, dentists have recently employed ceramics for restoration materials. Among the ceramic materials, zirconia provides high toughness and crack resistant characteristics. Residual stresses develop in processing due to factors including grain anisotropy and thermal coefficient mismatch. In the present study, polychromatic X-ray (Laue) micro...

Micro X-ray fluorescence ~MXRF! offers the analyst a new approach to materials characterization. The range of applications is expanding rapidly. Single point analysis has been demonstrated for nanoliter volumes with detection limits at the 0.5 ng level. MXRF can be used as an element specific detector for capillary electrophoresis. Elemental imaging applications include analysis of sample corro...

Bioglass-graphene oxide composites can be served as a high-potential candidate for biomedical applications due to its specific mechanical properties. In this study, the 45S5 bioactive glass (BG) - graphene oxide (GO) composite containing 2 wt. % GO was coated on titanium alloy via electrophoretic deposition process (EPD). The synthesized GO was incorporated into BG coating to improve the mechan...

in this work, a bench-scale process was developed using mineral-processing methods to recover iron from a placer deposit located in bardaskan, khorasan-e-razavi, iran. the mineralogical studies were performed by x-ray diffraction (xrd), x-ray fluorescence (xrf), electron probe micro-analyzer (epma), and an optical microscope. these studies indicated that titanomagnetite, magnetite, and hematite...

Combined microscopic X-ray fluorescence/microscopic X-ray diffraction (μ-XRF/μ-XRD) tomography is a recently developed method that allows the visualization of the distribution of chemical elements and the associated crystalline phases inside complex, heterogeneous materials of extended thickness (millimeter range) in a nondestructive fashion. In this paper, the accuracy and resolution with whic...