a very simple, rapid and sensitive dispersive liquid-liquid microextraction (dllme) followed by gas chromatography and flame ionization detection (gc-fid) was developed for the determination of phenol and carvacrol in honey samples. a mixture of 100 µl dichloromethane (extraction solvent) and 0.5 ml acetonitrile (disperser solvent) was rapidly injected into sample solution. thereby a cloudy sol...

RATIONALE In clinical trials, homogeneous emphysema patients have responded well to upper lobe volume reduction but not lower lobe volume reduction. MATERIALS/METHODS To understand the physiological basis for this observation, a computer model was developed to simulate the effects of upper and lower lobe lung volume reduction on RV/TLC and lung recoil in homogeneous emphysema. RESULTS Patie...

BACKGROUND The aims of this study are to investigate the difference between the diaphragm thickness at end expiration and the thickness at total lung capacity (TLC), and to examine differences in inspiratory muscle function between stroke patients and healthy individuals. MATERIAL AND METHODS Forty-five stroke patients and 49 healthy volunteers were included in this study. Diaphragm thickness w...

PURPOSE Lung size mismatch is a major cause of poor lung function and worse survival after lung transplantation (LTx). We compared predicted total lung capacity (pTLC) and TLC measured by chest computed tomography (TLC(CT)) in LTx candidates. MATERIALS AND METHODS We reviewed the medical records of patients on waiting lists for LTx. According to the results of pulmonary function tests, patien...

Radioimmunoassay (RIA) and thin-layer chromatography (TLC) were compared for morphine detection in an actual narcotic clinic setting. A choice of urines from all those screened by TLC allowed a critical comparison as to actual use or non-use of narcotic drugs, rather than a sampling at random in which the question of possible false positives or negatives cannot be conclusively answered. Althoug...

Thin-layer chromatography (TLC) has been a useful tool in the analysis of numerous urinary constituents; as in most applications of adsorption TLC, it is best used in conjunction with other chromatographic processes. The application of TLC to the resolution of polar urinary products derived from lipids is shown for the metabolism of a 14C-labeled fatty acid and a 14C-labeled glyceryl thioether....

Commercial precoated thin-layer chromatography (TLC) and highperformance TLC (HPTLC) plates with spherical or irregular particles have been compared on the basis of theoretical plate number (N), resolution (R), linearity, development time, and limit of sensitivity for analysis of a multicomponent analgesic tablet in the fluorescence quenching mode and analysis of a five-component dye mixture in...

We report the use of TLC image analysis software, JustTLC, for identification and quantitative evaluation of the photoproducts generated by the irradiation of Chlorpromazine water solutions with a 266 nm laser beam. The percent concentrations resulting for photoproducts from TLC analysis were compared with the relative concentrations of those identified by LC-TOF/MS measurements. The spots on t...

Kaempferia parviflora Wall. ex Baker is a medicinal plant found in the upper Northeastern regions of Thailand, which belongs to Zingiberaceae family. The present study aims to investigate the standardization parameters, to analyze chemical constituents of volatile oil by gas chromatography-mass spectrometry, and to determine the content of 5,7-dimethoxyflavone in K. parviflora rhizomes by thin-...