Controlled shape and size with tuneable band gap (1.92-2.41 eV), nickel sulphide NPs was achieved in presence of thiourea or thioacetamide as sulphur sources with the variations of temperature and capping agents. Synthesized NPs were fully characterized by powder XRD, IR, UV-vis, DRS, FE-SEM, TEM, EDX, XPS, TGA and BET. Capping agent, temperature and sulphur sources have significant role in con...

Novel multi-SO3H functionalized strong Brønsted acidic ionic liquid coated magnetite nanoparticles have been prepared and applied as catalyst for the synthesis of 2,4,5-trisubstituted imidazoles. The results showed that a novel catalyst was very efficient for the reaction and could be magnetically separated and reused at least 6 times with less reduction in its catalytic activity. Operational s...

Iron doped hexagonal mesoporous silica (Fe-HMS) was successfully prepared by one-pot direct synthesis at ambient temperature by using dodecylamine as a templating agent. The catalyst has been characterized by various techniques including XRD, DR-UV-Vis, FTIR, SEM and N2 adsorption. The obtained material exhibits very large surface area (above 1000 m(2) g(-1)), mesoporosity with narrow distribut...

Titanium dioxide (TiO(2)) nanofibers in the anatase structure were successfully prepared via electrospinning technique followed by calcination process. The morphologies, crystal structure, surface area, and the photocatalytic activity of resulting TiO(2) nanofibers were characterized by field emission scanning electron microscopy (FE-SEM), transmission electron microscopy (TEM), X-ray diffracti...

In this paper, a novel nanophosphor, Y10W2O21:Eu, was synthesized through co-precipitation which is a simple and low-costing method. The structure and morphology of the nanocrystal samples were characterized by using XRD and FE-SEM. The emission spectra, excitation spectra and fluorescence decay curves were measured. J-O parameters, quantum efficiencies of Eu3+ 5D0 energy level, color coordinat...

Zinc oxide is known as a promising material for sensing devices due to its piezoelectric properties. In particular, the alignment of ZnO nanostructures into ordered nanoarrays is expected to improve the device sensitivity due to the large surface area which can be utilized to capture significant quantities of gas particles. However, ZnO nanorods are difficult to grow on the quartz substrate wit...

In order to effectively photodegradate organic pollutants, ZnO composite and Co-B codoped TiO₂ films were successfully deposited on glass substrates via a modified sol-gel method and a controllable dip-coating technique. Combining with UV-Vis diffuse reflectance spectroscopy (DRS) and photoluminescence spectra (PL) analyses, the multi-modification could not only extend the optical response of T...

Novel uniform single-crystal boehmite leaf-like nanosheets with high anisotropy (with a lateral size of (4.5±0.5 μm)×(9.0±1.0 μm) and a thickness of 60–90 nm) and flower-like superstructures consisting of single-crystal petals were synthesized for the first time by a simple hydrothermal method. After calcination, those boehmite structures can be transformed into single-crystal gamma-alumina nan...

Activated carbon monoliths (ACMs) were fabricated by H2O activation using powdered fast pyrolytic char (PFPC) as a raw material and bio-oil phenol-formaldehyde (BPF) resin as a binder. The effects of the ratio of BPF resin to PFPC on textural and chemical-surface properties of the ACMs were investigated using elemental analysis, X-ray diffraction (XRD), Fourier transform infrared spectroscopy (...