Magnetic powder of Sr-ferrite was prepared by conventional and sol-gel auto-combustion methods. In conventional method, strontium carbonate and ferric oxide powders were mixed together and then mixture was calcined. In sol-gel auto-combustion method, a solution containing strontium nitrate, ferric nitrate and citric acid was heated until the combustion took place automatically; then, as-burnt p...

nanocrystalline particles of barium hexaferrite has been prepared by the sol–gel auto- combustion method using iron and barium nitrate with a ba:fe molar ratio of 1:10. the effect of fuel such as citric acid and aspartic acid was investigated on the structure and magnetic properties of nanoparticles. the results revealed that the formation of barium hexaferritefine particles is influenced by mo...

nanocrystalline zro2 with particle size of about 38 nm was directly synthesized by sol-gel auto-combustion method. the overall process involved three steps: formation of homogeneous sol at 50-55°c; formation of dried gel at 110°c, and combustion of the dried gel at 400°c. experiments revealed that zro2 dried gel derived from glycine (fuel) and nitrate sol exhibited self propagating combustion a...

zro2 nanopowder was prepared by the sol-gel auto-combustion method. the product was characterized by x-ray diffraction (xrd), energy dispersive analysis of x-ray (edx) and scanning electron microscopy (sem). the average crystalline size of zro2 was obtained 62 nm. also, photocatalytic removal of nitrophenol from aqueous solution by using nanoscale zro2 under uv light irradiation was studied. th...

sol–gel auto-combustion is a unique combination of the combustion and the chemical gelation processes. in this work, nanosize (d) powders with compositions of znfe2o4 were synthesized by sol–gel combustion method. the puffy, porous brown powders as-combusted was calcined at the temperature of 750–1000◦c for 4 h. these powders are characterized by x-ray diffraction and scanning electron microsco...

Nanocrystalline ZrO2 with particle size of about 38 nm was directly synthesized by sol-gel auto-combustion method. The overall process involved three steps: formation of homogeneous sol at 50-55°C; formation of dried gel at 110°C, and combustion of the dried gel at 400°C. Experiments revealed that ZrO2 dried gel derived from glycine (Fuel) and nitrate sol exhibited self pr...

zno and zro2 photo catalysts were synthesized by sol-gel auto combustion method. the products were characterized by x-ray diffraction (xrd) and scanning electron microscopy (sem). structural and morphological properties of nano particles were investigated and the average crystalline size of zno and zro2 was obtained 44 and 51 nm, respectively. also, photo catalytic degradation of nitro phenol f...

Nanocrystalline ZrO2 with particle size of about 38 nm was directly synthesized by sol-gel auto-combustion method. The overall process involved three steps: formation of homogeneous sol at 50-55°C; formation of dried gel at 110°C, and combustion of the dried gel at 400°C. Experiments revealed that ZrO2 dried gel derived from glycine (Fuel) and nitrate sol exhibited self pr...

It is well known that in recent years magnetic materials have received increased attention due to their properties. For this reason a significant number of patents that were published during the last decade are oriented towards synthesis and study of such materials. The aim of this work is to create and study ferrite nanocrystalline materials with spinel structure, using sol-gel technology with...

In this paper, strontium ferrite (SrO.6Fe2O3) was synthesized by the sol-gel auto-combustion process. The thermal behavior of powder obtained from self-propagating combustion of initial gel was evaluated by simultaneous differential thermal analysis (DTA) and thermo gravimetric (TG), from room temperature to 1200°C. The as-burnt powder was calcined at various temperatures from 700-900°C to achi...