a chelating resin of polystyrene divinylbenzene resin functionalized by 1-(2-pyridylazo) 2- naphtol (psdvb-pan) has been synthesized and its sorption properties have been investigated for preconcentration and determination of cadmium at μg/l level by flame atomic absorption spectrometry. the procedure is based on the sorption of cd(ii) ions on a minicolumn of synthesized chelating resin. the...

Several elements (V, Mo, Fe, Mn, Cd, Zn) as metallic impurities in pure uranium compounds were quantitatively determined by atomic absorption spectrometry. The effects of uranium and that of other factors on the absorption intensity of each element were studied. The analyzed samples were dissolved in 6 M nitric acid, and uranium was selectively extracted with tributylphosphate. The aqueous solu...

dispersive liquid-liquid microextraction technique based on solidification of a floating organic drop (dllme-sfo) combined with flame atomic absorption spectrometry was developed for determination of thallium in water sample. an appropriate mixture of acetone and 1-undecanol was rapidly injected into an aqueous sample containing tlcl4- which forms an ion pair with brilliant green reagent and as...

a chelating resin of polystyrene divinylbenzene resin functionalized by 1-(2-pyridylazo) 2- naphtol (psdvb-pan) has been synthesized and its sorption properties have been investigated for preconcentration and determination of cadmium at μg/l level by flame atomic absorption spectrometry. the procedure is based on the sorption of cd(ii) ions on a minicolumn of synthesized chelating resin. the re...

an efficient, rapid, simple, and highly selective dispersive liquid–liquid microextraction basedon solidification of floating organic drop (dllme-sfod), combined with flame atomicabsorption spectrometry was developed for preconcentration and determination of trace amountsof cobalt in water samples. in this method, an appropriate mixture of acetone and1-undecanol was injected rapidly into the aq...

Dispersive Liquid-Liquid MicroExtraction technique based on Solidification of a Floating Organic drop (DLLME-SFO) combined with flame atomic absorption spectrometry was developed for determination of thallium in water sample. An appropriate mixture of acetone and 1-undecanol was rapidly injected into an aqueous sample containing TlCl4- which forms an ion pair with bril...

Formation of the hydrides of antimony arsenic, bismuth, germanium, lead, selenium, tellurium and tin by reaction with sodium tetrahydroborate0 affords an excellent method for the separation of these elements as gases from a wide range of matrices. Excellent low limits of detection are attained when this separation method is combined with atomisation of the hydride in a heated quartz tube in the...

a simple and rapid microextraction procedure based on dispersive liquid-liquid microextraction (dllme) was developed for determination and speciation of trace amounts of chromium (cr) by flame atomic absorption spectrometry (faas). in the proposed approach, chloroform and methanol were used as extraction and dispersive solvents. a new schiff's base ligand, bis(2-methoxy benzaldehyde) ethylene d...

pb and cd in water samples were determined by cloud point extraction (cpe) with sodiumdiethyldithiocarbamate (ddtc) as the chelating agent and octylphenoxypolyethanl (triton x-114) asthe surfactant prior to flame atomic absorption spectrometry (faas) determination. the main factorsof affecting the extraction and detection processes were optimized. the preconcentration of 10 ml ofstandard soluti...

2. Referenced Documents 2.1 ASTM Standards: D1318 Test Method for Sodium in Residual Fuel Oil (Flame Photometric Method) D3237 Test Method for Lead in Gasoline by Atomic Absorption Spectroscopy D3340 Test Method for Lithium and Sodium in Lubricating Greases by Flame Photometer D3605 Test Method for Trace Metals in Gas Turbine Fuels by Atomic Absorption and Flame Emission Spectroscopy D3831 Test...