Chromatographic fractionation of crude extracts (C8 extracts) from the protein-enriched flour of commercial field peas (Pisum sativum L.) has been shown here to yield peptide mixtures related to the pea albumin 1b (PA1b) family of cysteine-rich plant peptides. The mixtures were obtained initially by flash chromatography with silica gel. Following elution of soyasaponins and lysolecithins, the e...

Two nonvolatile beta-carboline alkaloids were isolated from the Maillard reaction between xylose and tryptophan by solvent extraction and flash silica gel column chromatography. Their structures were elucidated by spectral methods (UV, MS, and NMR) as 1-(1,4-dihydroxybutyl)-beta-carboline and 1-(1,3, 4-trihydroxybutyl)-beta-carboline.

A single pot conversion of carboxylic acids into the corresponding 4-chlorobutyl esters has been achieved by a novel procedure. The intermediate acid chlorides are not isolated. The double bond and aromatic methoxy group survive the mild reaction conditions. In almost all the examples studied the products are purified by simple flash chromatography.

Tecoma stans is an ornamental perennial tropical and subtropical plant belonging to the Bignoniaceae family with green leaves yellow attractive fragrance flowers commonly known as trumpetbush or bells. The originated in areas of South America Mexico has been cultivated many countries such Egypt, Iraq, United Arab Emirates (UAE). T. found different parts UAE Ras Al Khaimah, Abu Dhabi, Dubai, whe...

High-throughput methods were applied to the production, analysis, and characterization of libraries of natural products in order to accelerate the drug discovery process for high-throughput screening in the pharmaceutical and biotechnology industries. Library production integrates automated flash chromatography, solid-phase extraction, filtration, and high-throughput parallel four-channel prepa...

In a previous study, selective degradation of carbohydrates versus lignin in buried woods was demonstrated by non-destructive spectroscopy (C NMR) and destructive wet chemical methods (acid hydrolysis and alkaline CuO oxidation). In this paper, spruce, alder and oak woods deposited in coastal sediments and their recent equivalents are characterized by pyrolysis-mass spectrometry and pyrolysis-g...