in this study, a simple and reliable method by gas chromatograph–mass spectrometry (gc–ms) was developed for the fast and regular identification of 3, 4-mdma impurities in ecstasy tablets. in so doing, 8 samples of impurities were extracted by diethyl ether under alkaline condition and then analyzed by gc–ms. the results revealed high mdma levels ranging from 37.6% to 57.7%. the gc-ms method sh...

background food born pathogenic bacteria are the most important agents of infections in humans, and food spoilage also results in economic losses in food industry. objectives the aim of this study was the evaluation of chemical components, total phenolic content, antioxidant and antibacterial activities of artemisia dracunculus essential oil. materials and methods the essential oil of tarragon ...

Gas chromatography-mass spectroscopy (GC-MS) is one of the so-called hyphenated analytical techniques. As the name implies, it is actually two techniques that are combined to form a single method of analyzing mixtures of chemicals. Gas chromatography separates the components of a mixture and mass spectroscopy characterizes each of the components individually. By combining the two techniques, an...

Inductively coupled plasma mass spectrometry is a powerful tool for the investigation of many materials. The Agilent 7500c with Octopole Reaction System was used to analyze major, minor and trace elements in two standard reference plant materials. The data obtained using the 7500c is compared to the certificate reference values and to results that were generated using inductively coupled plasma...

Gas chromatography (GC) is a widely applied technique in many branches of science and technology. For over half a century, GC has played a fundamental role in determining how many components and in what proportion they exist in a mixture. However, the ability to establish the nature and chemical structure of these separated and quantified compounds is ambiguous and reduced, and requires a spect...

background: the present study was the first attempt for determination and measurement of pesticide residues in tomatoes used in salad production plants in isfahan, central iran. methods: a multiresidue method based on modified quechers (quick, easy, cheap, effective, rugged and safe) sample preparation, followed by gas chromatography mass spectrometry (gc–ms) was developed and validated for the...

background: infectious diarrhoea is an emergent problem in both developing and developed countries for high rates of mortality in infants. in recent years, drug resistance to microbial pathogens has been commonly reported from all over the world. medicinal plants represent a rich source of antimicrobial agents. plants are used medicinally in different countries especially in india and are a sou...

background and objectives: in the production process of foods rich in carbohydrates and some other foods containing precursors of acrylamide formation, there is the possibility of acrylamide creation, which is a mutagen and carcinogen material. this study aims to introduce and optimize a new method for determining acrylamide in potato chips using xanthydrol as a derivative representative with g...