نتایج جستجو برای: hydrazine hydrate

تعداد نتایج: 9812  

2008
DenthajeKrishna Bhat

ZnO nanorods have been successfully synthesized by a simple microwave-assisted solution phase approach. Hydrazine hydrate has been used as a mineralizer instead of sodium hydroxide. XRD and FESEM have been used to characterize the product. The FESEM images show that the diameter of the nanorods fall in the range of about 25–75 nm and length in the range of 500–1,500 nm with an aspect ratio of a...

2009
You-Lei Zhang Yu-Jun Wu Guo Peng Hong Deng

The reaction of 2-carboxy-benzaldehyde and hydrazine hydrate unexpectedly yielded the title compound, C(16)H(10)N(2)O(3), which comprises one phthalide ring, one phthalazine system and a chiral centre. The phthalide unit is almost perpendicular to the phthalazine system, forming a dihedral angle of 87.1 (3)°. The packing is governed by weak C-H⋯O hydrogen-bonding inter-actions, forming layers p...

Journal: :Dalton transactions 2015
R Haiges G Bélanger-Chabot S M Kaplan K O Christe

Neat 3,5-dinitro-1H-1,2,4-triazole was obtained in quantitative yield from potassium 3,5-dinitro-1,2,4-triazolate and sulfuric acid. The compound was purified by sublimation in vacuo at 110 °C. Pure HDNT is a hygroscopic white solid that is impact and friction sensitive and decomposes explosively upon heating to 170 °C. However, the presence of impurities might lower the decomposition temperatu...

2010
Ebraheem Abdu Musad Kuriya Madavu Lokanatha Rai Kullaiah Byrappa

The new 3,5-(substituted) pyrazoles and isoxazoles were prepared by reaction of (N'(1)E, N'(3)E)- N'(1), N'(3)-bis (3,4,5-substitutedbenzylidene)malonohydrazide with hydrazine hydrate and hydroxylamine hydrochloride respectively under solvothermal conditions involving an ecofriendly method without any environmental pollution, the yield are in the range of 75-96%. The structure of the new compou...

Journal: :Chemical communications 2010
Baojiang Jiang Chungui Tian Lei Wang Yuanxiang Xu Ruihong Wang Yingjie Qiao Yuguang Ma Honggang Fu

High quality graphenes were prepared from low-cost expandable graphite via a facile hydrazine hydrate or concentrated ammonia-assisted quenching strategy.

Journal: :The journal of physical chemistry. B 2006
Qilong Liao Rina Tannenbaum Zhong Lin Wang

The present paper presents a facile and low-cost hydrothermal method to synthesize stoichiometric FeNi3 alloy nanoparticles by reducing Ni(NO3)2.6H(2)O and Fe(NO3)2.9H(2)O with hydrazine hydrate in strong alkaline media. X-ray diffraction patterns of as-prepared samples synthesized at 180 degrees C for different hydrothermal reaction times reveal that the products are pure stoichiometric FeNi3 ...

2010
Shi-Quan Chen Kai Jiang Shi-Fan Wang

The title compound, C(10)H(11)N(3)O(3), was synthesized by the reaction of 3,5-bis-(ethoxy-carbon-yl)-2-formyl-4-methyl-1H-pyrrole and hydrazine hydrate. The angle between the pyrrole ring and the pyridazinone ring is 0.93 (9)°. In the crystal, inter-molecular N-H⋯O and N-H⋯N hydrogen-bond inter-actions link the mol-ecules into a two-dimensional network.

2009
Qing-Peng He Hong-Gang Li Guang-Bo Wang Feng-Lian Fu Ming-Shi Liu

The title compound, 3C(14)H(12)N(2)O(2)·C(3)H(7)NO, was synthesized by reaction of benzoyl chloride with hydrazine hydrate under microwave irradition. The asymmetric unit comprises three 1,2-dibenzoyl-hydrazine mol-ecules and one dimethyl-formamide mol-ecule. The 1,2-dibenzoyl-hydrazine mol-ecules are linked by pairs of N-H⋯O hydrogen bonds into chains propagating along [010].

2016
Jeongmo Kim Wilson Jose da Silva Abd. Rashid bin Mohd Yusoff Jin Jang

Herein, we demonstrate a facile approach to synthesize long nickel nanowires and discuss its suitability to replace our commonly used transparent electrode, indium-tin-oxide (ITO), by a hydrazine hydrate reduction method where nickel ions are reduced to nickel atoms in an alkaline solution. The highly purified nickel nanowires show high transparency within the visible region, although the sheet...

Journal: :Nano letters 2008
Jeremy T Robinson F Keith Perkins Eric S Snow Zhongqing Wei Paul E Sheehan

We demonstrate reduced graphene oxide as the active material for high-performance molecular sensors. Sensors are fabricated from exfoliated graphene oxide platelets that are deposited to form an ultrathin continuous network. These graphene oxide networks are tunably reduced toward graphene by varying the exposure time to a hydrazine hydrate vapor. The conductance change of the networks upon exp...

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