Cetyltrimethyl ammonium bromide cationic (CTAB) surfactant was used as template for the synthesis of nanoclusters of ZnS composed of nanowires, by hydrothermal method. The structural and morphological studies were performed by using X-ray diffraction (XRD), scanning electron microscopy (SEM) and high resolution transmission electron microscopy (HRTEM) techniques. The synthesized ZnS nanocluster...

A new ethylenediaminetetraacetic acid- (EDTA-) mediated hydrothermal route to prepare chrysanthemum-shaped samarium orthovanadate (SmVO₄) nanocrystals with decavanadate (K₆V₁₀O₂₈·9H₂O) as vanadium source has been developed. The present hydrothermal approach is simple and reproducible and employs a relatively mild reaction temperature. The EDTA, pH value, and temperature of the reaction systems ...

MnO2 materials are prepared through a hydrothermal process. Sn-doping and composite graphene are both achieved simultaneously during the hydrothermal reaction then obtain the electrode materials of supercapacitors. Morphology, structure and electrochemical properties of the samples are evaluated by X-ray diffraction(XRD), scanning electron microscopy (SEM), and electrochemical work station. The...

nano-zeolite coapo-5 as a member of afi family, was synthesized via a hydrothermal treatment, and structurally characterized using x-ray diffraction (xrd), scanning electron microscope (sem), and energy dispersive x-ray analysis (edax). the effects of crystallization temperature and time on the structure of these powder products were studied. xrd patterns of the synthesized powders revealed a h...

in this study, the tio2 nanorods were synthesized from p25 tio2 nanoparticles by hydrothermal method in 10 m naoh solution. the effects of annealing temperatures on produced nanorods were investigated  by scanning  electron microscopy (sem) x-ray diffraction (xrd) and photoluminescence (pl) spectroscopy. diameter growth and  changes  of  surface  oxygen  defects of  synthesized nanorods are stu...

Demonstrated herein is a single rapid approach employed for synthesis of Ag-graphene nanocomposites, with excellent antibacterial properties and low cytotoxicity, by utilizing a continuous hydrothermal flow synthesis (CHFS) process in combination with p-hexasulfonic acid calix[6]arene (SCX6) as an effective particle stabilizer. The nanocomposites showed high activity against E. coli (Gram-negat...

SrF2:Eu,Ce3+ nanophosphors were successfully synthesized by the hydrothermal method during down-shifting investigations for solar cell applications. The phosphors were characterized by X-ray diffraction (XRD), scanning Auger nanoprobe, time of flight-secondary ion mass spectrometry (TOF-SIMS), X-ray photoelectron spectroscopy (XPS) and photoluminescence (PL) spectroscopy. XRD showed that the cr...

Spherical MCM-48 mesoporous sieve co-doped with vanadium and iron was successfully synthesized via one-step hydrothermal method. The material was characterized by X-ray diffraction (XRD), nitrogen adsorption-desorption isotherms, inductively coupled plasma (ICP), scanning electron microscopy (SEM), transmission electron microscopy (TEM), diffuse reflectance UV-vis spectra, and X-ray photoelectr...

Metal oxides play significant role in many fields of nanotechnology including nanocatalysis, sensing, supermagnetic properties, fuel cells, nanoenergy storage and conservation. Dyes are synthetic compounds which have wide range of application in textiles, paints etc., and the dye effluents from the dyeing industries cause water pollution. In this present study, ZnO photocatalyst have been synth...

cobalt ferrite nano-powder have been obtained through a hydrothermal method with 2:1 molar ratio of fe:co without using any surfactant. x-ray diffraction (xrd) and scanning electron microscopy (sem) were used to consider the structural and morphological properties of cofe2o4 nano-particles. also, edax spectroscopy applied to evaluate the chemical composition. results demonstrated that 15 hr hyd...