نتایج جستجو برای: liquid phase micro extraction

تعداد نتایج: 1024711  

Daruish Badakhshan, Majid Ramezani,

Background: A syringe to syringe dispersive liquid phase micro-extraction-floating organic drop was applied and used for the simultaneous extraction and pre-concentration of trace amounts of amphetamine (AMP) and methamphetamine (MAMP) in urine samples. The extracted analytes were determined by high performance liquid chromatography along with diode array detection. Materials & Methods: In thi...

2017
Abuzar Kabir Marcello Locatelli Halil Ibrahim Ulusoy

Sample preparation has been recognized as a major step in the chemical analysis workflow. As such, substantial efforts have been made in recent years to simplify the overall sample preparation process. Major focusses of these efforts have included miniaturization of the extraction device; minimizing/eliminating toxic and hazardous organic solvent consumption; eliminating sample pre-treatment an...

2016
Jie Peng Fang Tang Rui Zhou Xiang Xie Sanwang Li Feifan Xie Peng Yu Lingli Mu

Biological sample pretreatment is an important step in biological sample analysis. Due to the diversity of biological matrices, the analysis of target substances in these samples presents significant challenges to sample processing. To meet these emerging demands on biopharmaceutical analysis, this paper summarizes several new techniques of on-line biological sample processing: solid phase extr...

Journal: :Talanta 2015
Ahmad Makahleh Hui Fang Yap Bahruddin Saad

A new, rapid and sensitive microextraction technique named vortex-assisted liquid-liquid-liquid microextraction (VALLLME) is proposed. The complete extraction process involves two steps. First, a vortex-assisted liquid-liquid microextraction (VALLME) procedure was used to extract the analytes from a relatively large volume of sample (donor phase) to a small volume of organic solvent (intermedia...

Journal: :analytical and bioanalytical chemistry research 2014
fariborz momenbeik faezeh tajmir riahi

in this project, eggshell membrane was used as a solid phase extraction sorbent for extraction of morphine followed by hplc analysis. at first, raw eggshell membrane was used and then, because of low adsorption of morphine on untreated eggshell membrane (

Journal: :journal of herbal drugs 0
majid mohammadhosseini department of chemistry, shahrood branch, islamic azad university, shahrood, iran

background & aim:nepeta racemosa is an herbal and medicinal plant and this report aims to   identify chemical compositions of the essential oils and volatiles of its   aerial parts through classical and advanced methods.  experimental: chemical profiles of the essential oils and volatile compounds from the aerial parts of nepeta racemosa obtained through hydrodistillation (hd), solvent-free mic...

Dispersive Liquid-Liquid Microextraction / Thermal Lens Microscopy (DLLME/TLM) was developed as a new combination method for preconcentration and determination of Cd. Thermal Lens Microscopy is suitable for the determination of analyte after DLLME because of the low volume of the remained phase after DLLME and increasing of the enhancement factor for the nonpolar organic solvents. Some effe...

Journal: :iranian journal of oil and gas science and technology 0
amir hosein tahershamsi m.s. student, department of chemical engineering, iran university of science and technology (iust), tehran, iran ahad ghaemi assistant professor of department of chemical engineering, iran university of science and technology (iust), tehran, iran mansour shirvani associate professor of department of chemical engineering, iran university of science and technology (iust), tehran, iran

in this study, liquid-liquid extraction process in a kuhni extraction column was modeled and simulated. a non-equilibrium dynamic model was developed for modeling liquid-liquid extraction processes based on a rate-based model. the model equations are inclusive of partial and ordinary differential equations which were discretized in column height direction. the population balance model was used ...

Journal: :journal of chemical health risks 0
aldo pacheco ferreira

the occurrence and fate of trace-level contamination of pharmaceuticals in the aquatic environment has been recognized as one of the emerging issues in environmental chemistry. the effluents of wastewater treatment plants, usually directly emitted to the environment, often contain the anti-inflammatory drug diclofenac. diclofenac was chosen because it is of high consumption; by background liter...

2003
A. Aota M. Nonaka

We demonstrated micro counter-current flow in a glass microchip utilizing surface modification patterning method to control surface tension. In order to visualize the micro counter-current flow, fluorescent microparticle dispersion solutions were observed by fluorescence microscopy. When the flow volume ratio of water and organic solution was changed, the switching point of flow direction was o...

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