We describe a sample-processing micro-reactor that utilizes 60 GHz RF radiation with approximately 730 mW of output power. The instrument design and performance characterization are described and then illustrated with modeling and experimental studies. The micro-reactor's efficiency on affecting hydrolysis of chemical bonds similar to those within large complex molecules was demonstrated: a dis...

The design, fabrication and performance of a novel and highly sensitive micro-reactor device for performing in situ grazing-incidence X-ray scattering experiments of model catalyst systems is presented. The design of the reaction chamber, etched in silicon on insulator (SIO), permits grazing-incidence small-angle X-ray scattering (GISAXS) in transmission through 10 µm-thick entrance and exit wi...

This study presents an optimal design of the coolant system a non-refueling full-life small reactor by analyzing space-integrated geometrical and electromagnetic variables extra vessel pump (EVEMP) for circulation lead–bismuth eutectic (LBE) coolant. The EVEMP is ideal alternative to thermal-hydraulic micro reactors as it possesses no internal structures, such impellors or sealing transportatio...

Small volume operation and rapid thermal cycling have been subjects of numerous reports in micro reactor chip development. Sensitivity aspects of the micro PCR reactor have not been studied in detail, however, despite the fact that detection of rare targets or trace genomic material from clinical and/or environmental samples has been a great challenge for microfluidic devices. In this study, a ...

in this study, the effect of the levels of hydrogen addition to methane-air premixed flame in a micro-stepped reactor has been studied numerically. in addition, the effects of mixture velocity and walls’ thermal conductivity (kw) on the flame’s location, temperature, and species distribution in a micro reactor were calculated using a 2d numerical laminar steady code. the results showed that an ...

micro scale gas flows has attracted significant research interest in the last two decades. in this research, the fluid flow of gases in the stepped micro-channel at a wide range of knudsen number has been analyzed with using the lattice boltzmann (mrt) method. in the model, a modified second-order slip boundary condition and a bosanquet-type effective viscosity are used to consider the velocity...

Deactivation of commercially relevant cobalt catalysts for Low Temperature Fischer-Tropsch (LTFT) synthesis is discussed with a focus on the two main long-term deactivation mechanisms proposed: Carbon deposits covering the catalytic surface and re-oxidation of the cobalt metal. There is a great variety in commercial, demonstration or pilot LTFT operations in terms of reactor systems employed, c...