A highly selective, sensitive, rapid and economical differential pulse polarographic method has been developed for the determination of trace amounts of antimony in various standard alloys and biological samples after adsorption of its 2-nitroso-1-naphthol-4-sulfonic acid - tetradecyldimethylbenzylammonium chloride on microcrystalline naphthalene in the pH range of 7.5-11.0. After filtratio...

a highly selective, sensitive, rapid and economical differential pulse polarographic method has been developed for the determination of trace amounts of antimony in various standard alloys and biological samples after adsorption of its 2-nitroso-1-naphthol-4-sulfonic acid - tetradecyldimethylbenzylammonium chloride on microcrystalline naphthalene in the ph range of 7.5-11.0. after filtration, t...

Mercury is quantitatively retained with 1, 5-diphenylcarbazone (DPC) on microcrystallinenaphthalene in the pH range 6.5-8.5 from a large volume of aqueous solutions of various samples.After filtration, the solid mass consisting of the mercury complex and naphthalene was dissolvedin 5.0 mL of dimethylformamide (DMF) and mercury was determined by spectrophotometricmethod at 542 nm against the rea...

Manganese is quantitatively retained on 2-(5-bromo-2-pyridylazo)-5-diethylaminophenol (5-Br-PADAP)-ammonium tetraphenylborate with microcrystalline naphthalene or by a column method in the pH range 7.5-10.5 from large volumes of aqueous solutions of various samples. After filtration, each solid mass consisting of the manganese complex and naphthalene was dissolved with 5 ml of dimethylformamide...

mercury is quantitatively retained with 1, 5-diphenylcarbazone (dpc) on microcrystallinenaphthalene in the ph range 6.5-8.5 from a large volume of aqueous solutions of various samples.after filtration, the solid mass consisting of the mercury complex and naphthalene was dissolvedin 5.0 ml of dimethylformamide (dmf) and mercury was determined by spectrophotometricmethod at 542 nm against the rea...

Vanadium is quantitatively retained on 2-nitroso-1-naphhthol-4-sulfonic acid tetradecyldimethlbenzyammonium chloride onto microcrystalline naphthalene in the pH range of 3.0-4.0 from a large volume of aqueous solutions of various alloys and synthetic samples. After filtration, the solid mass consisting of the vanadium complex and naphthalene was dissolved with 5.0 mL of dimethylformamide an...

A highly selective, sensitive, rapid and economical differential pulse polarographic method has been developed for the determination of trace amounts of cadmium in various samples after the adsorption of its 1-(2-pyridylazo)-2-naphthol (PAN) complex on microcrystalline naphthalene in the pH range of 8.2-11.0. After filtration, the solid mass is shaken with 9.0 mL of 1 M hydrochloric acid and ca...

Osmium was determined spectrophotometrically after coprecipitation with 5-chloro-2-hydroxythiobenzhydrazide at room temperature in the pH range 2.5-5.0 and collection on microcrystalline naphthalene. Beer's law was obeyed in the concentration range 1.8-14.4 ppm of osmium in a chloroform solution at 510 nm. The molar absorptivity and Sandell sensitivity were 1.056 x 10(4) l mol(-1) cm(-1) and 0....