A pressurized capillary electrochromatographic (pCEC) fingerprint of Ginkgo biloba leaf extract was developed on three different types of capillary columns. A commercial column packed with 3-microm particles and an in-house column packed with 5-microm particles were investigated for their performance. Additionally, a monolithic column was included in the fingerprint study as a potential alterna...

Duplex capillary columns with a packed and an open section are widely used in electrochromatography (CEC). The duplex column configuration leads to non-uniform voltage drop, electrical field distribution and separation performance. It also adds to the complexity in understanding and optimizing electrochromatographic process. In this study, we introduced a simplex column configuration based on s...

We developed a packed-column chromatographic procedure capable of simultaneous quantitation of methanol, ethanol, isopropanol, acetone, and ethylene glycol. This method was then updated to a rapid, sensitive, wide-bore capillary method. The packed-column system uses direct injection of 1 microL of Na2WO4/H2SO4-deproteinized serum onto a 1.8 m x 2 mm (i.d.) column packed with 80/100 HayeSep R. A...

iron is quantitatively retained on an adsorbent made by coprecipitation of 1,2-dihydroxybenzene-3,5-disulfonic acid (tiron) and tetradecyldimethylbenzylammonium choride (tdba) an microcrystalline naphthalene as a slurry or packed in a column, in the ph range 6.0-9.0 from a large volumes of aqueous solutions (up to 200 ml on microcrystalline naphthalene and up to 500 ml of aqueous solutions in t...