: A new fibrous adsorbent was prepared by grafting Acrylic Acid /Acryl Amide (AA/AAm) co-monomers onto Poly(Ethylene Terephtalat) (PET) fibers. The resulting sorbent has been characterized by Fourier Transform InfraRed spectroscopy (FT-IR), Thermo Gravimetric Analysis (TGA), Scanning Electron Microscopy (SEM) and elemental analysis and studied for the preconcentration and ...

The base-catalyzed Michael addition of 2-methyl-acryl-amide to benzotriazole afforded 3-(1H-benzotriazol-1-yl)-2-methyl-propanamide, C10H12N4O (1), in 32% yield in addition to small amounts of isomeric 3-(2H-benzotriazol-2-yl)-2-methyl-propanamide, C10H12N4O (2). In a similar manner, 3-(1H-benzotriazol-1-yl)-N,N-di-methyl-propanamide, C11H14N4O (3), was prepared from benzotriazole and N,N-di-me...

The title compound, C(15)H(24)N(2)O(2), crystallizes with two unique mol-ecules, (I) and (II), in the asymmetric unit, differing in the orientation of the acryloyl units with respect to the piperidine rings. The acryl-amide units are essentially planar in both mol-ecules (r.m.s. deviations = 0.042 and 0.024 Å, respectively), as are the C(3)N chains of the acryloyl units. The carbonyl O atoms of...

The title compound, C24H31NO3 {systematic name: (E)-3-[(1R*,2S*,4aS*,8aR*)-2-(benzo[d][1,3]dioxol-5-yl)-1,2,4a,5,6,7,8,8a-octa-hydro-naphthalen-1-yl]-N-iso-butyl-acryl-amide}, is a natural product isolated from the stem bark of B. obscura. It is composed of an octa-hydro-naphthalene ring system substituted with an essentially planar benzodioxole ring system [r.m.s. deviation = 0.012 Å] and an e...

two new samples of poly(amide-imide)/nanocomposites containing bicyclo segment and dibenzalaceton moiety in the main chain were synthesized by a solution intercalation technique. poly(amide-imide) (pai) 8 as a source of polymer matrix was synthesized by the direct polycondensation reaction of n,n´-bis(4-carboxyphenyl)bicyclo[2,2,2]oct-7-ene-2,3,5,6-tetracarboxylic diimide 3 with 2,6-bis(4-amino...

The mol-ecule of the title compound [systematic name: N-(carbamoylmeth-yl)prop-2-enamide], C(5)H(8)N(2)O(2), which can be radically polymerized to polymers with thermoresponsive behavior in aqueous solution, consists of linked essentially planar acryl-amide and amide segments [maximum deviations = 0.054 (1) and 0.009 (1) Å] with an angle of 81.36 (7)° between their mean planes. In the crystal, ...

The aim of this present study was to develop a pH sensitive interpenetrating polymeric network (IPN) hydro gels (HG) based on chitosan-acryl amide-grafted-poly ethylene glycol (CTS-AM-PEG) followed by hydrolysis that are cross-linked with glutaraldehyde (GA). Cefotaxime is an antibiotic drug was successfully loaded in these IPNHG’s. The HGs formed were characterized by Fourier transform infrare...

hydrogels, due to their unique potentials such as high-water content and hydrophilicity are interest for the controlled release of drug molecules. the present study aims to create a controlled-release system through the preparation and characterization of hydrogels based on ph-sensitive polymers such as poly (acrylic acid). poly (acrylic acid), p(aa), hydrogel has been synthesized by radical po...