zno and zro2 photo catalysts were synthesized by sol-gel auto combustion method. the products were characterized by x-ray diffraction (xrd) and scanning electron microscopy (sem). structural and morphological properties of nano particles were investigated and the average crystalline size of zno and zro2 was obtained 44 and 51 nm, respectively. also, photo catalytic degradation of nitro phenol f...

Nanocrystalline ZrO2 with particle size of about 38 nm was directly synthesized by sol-gel auto-combustion method. The overall process involved three steps: formation of homogeneous sol at 50-55°C; formation of dried gel at 110°C, and combustion of the dried gel at 400°C. Experiments revealed that ZrO2 dried gel derived from glycine (Fuel) and nitrate sol exhibited self pr...

Nanocrystalline complex oxides have been synthesized by combination of sol–gel auto combustion and ultrasonic irradiation techniques using copper nitrate, zinc nitrate as metallic nitrates and glycine, urea and thiourea as fuels. Sol-gel combustion (combination of the chemical sol–gel process and the combustion process) as a proper synthesized technique is used to synthesize ZnO/CuO nanocomposi...

Nanocrystalline complex oxides have been synthesized by combination of sol–gel auto combustion and ultrasonic irradiation techniques using copper nitrate, zinc nitrate as metallic nitrates and glycine, urea and thiourea as fuels. Sol-gel combustion (combination of the chemical sol–gel process and the combustion process) as a proper synthesized technique is used to synthesize ZnO/CuO nanocomposi...

In this paper, strontium ferrite (SrO.6Fe2O3) was synthesized by the sol-gel auto-combustion process. The thermal behavior of powder obtained from self-propagating combustion of initial gel was evaluated by simultaneous differential thermal analysis (DTA) and thermo gravimetric (TG), from room temperature to 1200°C. The as-burnt powder was calcined at various temperatures from 700-900°C to achi...

Sol–gel auto-combustion is a unique combination of the combustion and the chemical gelation processes. In this work, nanosize (d) powders with compositions of ZnFe2O4 were synthesized by sol–gel combustion method. The puffy, porous brown powders as-combusted was calcined at the temperature of 750–1000◦C for 4 h. These powders are characterized by X-ray diffraction and scanning electron microsco...

Sol–gel auto-combustion is a unique combination of the combustion and the chemical gelation processes. In this work, nanosize (d) powders with compositions of ZnFe2O4 were synthesized by sol–gel combustion method. The puffy, porous brown powders as-combusted was calcined at the temperature of 750–1000◦C for 4 h. These powders are characterized by X-ray diffraction and scanning electron microsco...

The composite powders of barium-magnesium ferrite were prepared using sol-gel auto-combustion and microwave methods. The crystal structure and the shape of nanocomposites have been compared. X-ray Diffraction (XRD), Scanning Electron Microscope (SEM) and Vibrating Sample Magnetometer (VSM) were used to investigate the structural, morphological and magnetic properties of nanopowder. The formatio...

the aim of this study is to evaluate the influence of ph on the synthesis of nanocrystallines cobalt ferrite by combination of sol- gel auto combustion and ultrasonic irradiation methods. two different fuels, urea and thiourea, along with metal nitrates (oxidant) were used to prepare cofe2o4 powders. the morphology of the resulting powders was investigated. the powders were characterized by x-r...

The composite powders of barium-magnesium ferrite were prepared using sol-gel auto-combustion and microwave methods. The crystal structure and the shape of nanocomposites have been compared. X-ray Diffraction (XRD), Scanning Electron Microscope (SEM) and Vibrating Sample Magnetometer (VSM) were used to investigate the structural, morphological and magnetic properties of nanopowder. The formatio...