نتایج جستجو برای: sol gel combustion technique
تعداد نتایج: 730294 فیلتر نتایج به سال:
Magnetic powder of Sr-ferrite was prepared by conventional and sol-gel auto-combustion methods. In conventional method, strontium carbonate and ferric oxide powders were mixed together and then mixture was calcined. In sol-gel auto-combustion method, a solution containing strontium nitrate, ferric nitrate and citric acid was heated until the combustion took place automatically; then, as-burnt p...
It is well known that in recent years magnetic materials have received increased attention due to their properties. For this reason a significant number of patents that were published during the last decade are oriented towards synthesis and study of such materials. The aim of this work is to create and study ferrite nanocrystalline materials with spinel structure, using sol-gel technology with...
nanocrystalline zro2 with particle size of about 38 nm was directly synthesized by sol-gel auto-combustion method. the overall process involved three steps: formation of homogeneous sol at 50-55°c; formation of dried gel at 110°c, and combustion of the dried gel at 400°c. experiments revealed that zro2 dried gel derived from glycine (fuel) and nitrate sol exhibited self propagating combustion a...
highly sinterable alumina nano-powders have been synthesized by a sol-gel combustion method with glycine asfuel. the preparation involved the thermal decomposition of a chelating agent (fuel)-nitrate gel and theformation of amorphous precursors. the nanopowders calcined at 1100°c were characterized by x-ray powderdiffraction (xrd) and scanning electron microscopy (sem). it was found that the ch...
nanocrystalline particles of barium hexaferrite has been prepared by the sol–gel auto- combustion method using iron and barium nitrate with a ba:fe molar ratio of 1:10. the effect of fuel such as citric acid and aspartic acid was investigated on the structure and magnetic properties of nanoparticles. the results revealed that the formation of barium hexaferritefine particles is influenced by mo...
Sol–gel auto-combustion is a unique combination of the combustion and the chemical gelation processes. In this work, nanosize (d) powders with compositions of ZnFe2O4 were synthesized by sol–gel combustion method. The puffy, porous brown powders as-combusted was calcined at the temperature of 750–1000◦C for 4 h. These powders are characterized by X-ray diffraction and scanning electron microsco...
zro2 nanopowder was prepared by the sol-gel auto-combustion method. the product was characterized by x-ray diffraction (xrd), energy dispersive analysis of x-ray (edx) and scanning electron microscopy (sem). the average crystalline size of zro2 was obtained 62 nm. also, photocatalytic removal of nitrophenol from aqueous solution by using nanoscale zro2 under uv light irradiation was studied. th...
Nanocrystalline ZrO2 with particle size of about 38 nm was directly synthesized by sol-gel auto-combustion method. The overall process involved three steps: formation of homogeneous sol at 50-55°C; formation of dried gel at 110°C, and combustion of the dried gel at 400°C. Experiments revealed that ZrO2 dried gel derived from glycine (Fuel) and nitrate sol exhibited self pr...
Sol–gel auto-combustion is a unique combination of the combustion and the chemical gelation processes. In this work, nanosize (d) powders with compositions of ZnFe2O4 were synthesized by sol–gel combustion method. The puffy, porous brown powders as-combusted was calcined at the temperature of 750–1000◦C for 4 h. These powders are characterized by X-ray diffraction and scanning electron microsco...
The sol–gel technique is a highly flexible technique for fabrication of oxide glasses, and various researchers have previously reported fluorescence studies of Er-doped sol–gel films and monoliths. Here we report the fabrication of Er-doped strip-loaded sol–gel silicate waveguides, using a silica–titania–alumina host composition, and Er concentrations up to f1.1=10 Er rcm, for possible applicat...
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