Abstract A recently proposed combination of headspace liquid-phase microextraction with an optical immersion probe (HS-LPME-OIP) was adapted for the spectrophotometric determination ammonium. The developed method is based on conversion ammonium ions to ammonia in a 0.15 M sodium hydroxide solution, followed by absorption 200 µL Nessler's reagent solution preliminary diluted distilled water (1:1...

The article considers a sorption method for extracting copper ions from model nitric acid solution based on of electrolytic refining silver with using sorbents bis-picolylamine functional groups: Dowex M-4195 and AXIONIT BPA. possibility to residual concentrations in the less than 10 mg/l is shown. working capacity both samples under batch conditions, as well dynamic exchange full ?onditions (c...

Highly pure and well-dispersed yttria nanocrystalline powders were synthesized with a modified coprecipitation method that uses mixed ammonium hydroxide-carbonate solution as the precipitant poly acrylic acid (PAA) dispersant. Comparing using same route but without PAA dispersant, PAA-assisted exhibit lower level of agglomeration better sinterability. Sintering trajectories dispersant investiga...

A new and non-infringing efficient one-pot process for the preparation of catechol-O- methyltransferase (COMT) enzyme inhibitors, entacapone 1 under mild condition, initially reaction 3-methoxy-4-hydroxy-5-nitro-benzaldehyde 5 with 2-cyano acetic acid 13 in presence organic base benzyl Trimethyl ammonium hydroxide, i.e. Triton-B which undergo Knoevenagel condensation to get intermediate 22 is t...

This paper deals with some basic proteins of cell nuclei which differ in a number of ways from the classical histones of Kossel. Two characteristics of a histone noted by Kossel are its high arginine content and its way of being precipitated on addition of an excess of ammonium hydroxide (1-2). A high arginine content would tend to give a protein a basic isoelectric point and precipitability in...

The objective of this study was to determine whether aging would alter the beneficial effects (tenderness, juiciness, and flavor) of enhancing beef chuck and round steaks with a 20% solution of water, ammonium hydroxide, salt, and carbon monoxide. A randomized, complete block design was used, with 2 treatments [0% (control) and 20% (pump)], 3 aging periods (1, 2, and 3 wk), 3 muscles (M. tricep...

Ammonium hydroxide (NH4OH) is a chemical used in the manufacture of semiconductor devices, and must therefore be analyzed for trace metal impurities. The direct analysis of undiluted (20%) NH4OH using ICP-MS is challenging, because its high vapor pressure causes plasma instability. However, dilution of the samples would degrade detection limits, so the ability to directly analyze 20% NH4OH is i...