Equal channel multi angular pressing (ECMAP) process is the efficient method to enhance the productivity of ultra-fine grained (UFG) materials, by increasing process continuity and as a result decreasing process required time. Comparing repetitive ECAP method, in the same period, the number of passes can be done by ECMAP. In this article, ECMAP of AL strips in two typical annealed and as receiv...

in this paper, a viscous flow simulation is presented using the lattice boltzmann equation (lbe). a finite volume approach is adapted to discretize the lbe on a cell-centered, arbitrary shaped, rectangular tessellation. the formulation includes upwind scheme and high order descretization schemes for the flux term and collision operator respectively. a consistent open and solid boundary treatmen...

Saikosaponin (SS) A is a compound with various pharmacological properties and is easily degraded into SS-B1 and SS-G under acid conditions. In the present work, two new degradation products of SS-A, formed under acid hydrolytic conditions, were detected and isolated using analytical and semi-preparative liquid chromatography technology; furthermore, their structures were characterized as hydrox...

Saikosaponin (SS) a is a compound with various pharmacological properties and easily degraded into SSb1 and SSg in acid condition. In present work another two new degradation products of SSa formed under acid hydrolytic condition were detected and isolated by analytical and semi-preparative liquid chromatography technology, furthermore their structures were characterized as hydroxyl-saikosaponi...

Uniform line spacing plane gratings are introduced into a recording system to generate aspherical wavefronts for recording varied line spacing plane holographic gratings. Analytical expressions of groove parameters are derived to the fourth order. A ray-tracing validation algorithm is provided based on Fermat's principle and a local search method. The recording parameters are optimized to recor...

Uncertainty associated to analytical results is an issue of major interest for the whole analytical community. A large effort has been made to improve analytical techniques and procedures aimed to achieve a well characterized uncertainty associated with analysis. However, it is becoming increasingly recognised that uncertainty deriving from sampling and subsampling can even dominate the global ...

OBJECTIVES The aim of this study was to develop a simpler and more rapid analytical method for unbound teicoplanin in serum. METHODS A new analytical method was developed by modifying an existing fluorescence polarization immunoassay (FPIA) method. The validation of the developed FPIA method was compared in the quantification of unbound teicoplanin with that of the high-performance liquid chr...

there is a great interest in developing rapid analytical methods and provide appropriate parametersfor quantitative analysis of compounds derived from refractory pollutants. such methods are important forroutine quality control analysis of an effluent before being discharged into the environment. therefore, a rapid methodology for identification and quantification of some aliphatic acids is pro...