The objective of this research was to develop, optimize, and validate a modern, rapid method of preparation of human hair samples, using microwave irradiation, for analysis of eight tricyclic antidepressants (TCADs): nordoxepin, nortriptyline, imipramine, amitriptyline, doxepin, desipramine, clomipramine, and norclomipramine. It was based on simultaneous alkaline hair microwave-assisted hydroly...

a pressurized fluid extraction (pfe) method for the extraction of pistachio oil was developed using a modified supercritical fluid extractor. the supercritical fluid extraction apparatus was modified to be able to pump liquid solvent and co2 into the extraction vessel alternatively. the experimental results showed that the extraction yield was independent of the extraction pressure. it was also...

A simple HPLC-UV method has been developed and validated for the quantification of ellagic acid (EA) in ethanol extracts of Eugenia uniflora L. (Myrtaceae) leaves. The ultrasound-assisted extraction (UAE) optimization was performed using a Box Behnken design (33) combined with response surface methodology to study the effects of the ethanol concentration (%, w/w), extraction time (minutes), and...

The purpose of this study was to extract phenolic compounds from olive leaves of Koroneiki, Roghani and Mission varieties by maceration and Microwave-assisted extraction (MAE) methods with different solvents. Our results revealed that the extraction method, solvent and variety had a significant effect on the amount of phenolic compounds (p<0.05). In both extraction methods, Koroneiki and Missio...

The aim of this work is to compare the extraction efficiencies of microwave and conventional isolation of mangiferin from Mangifera indica L. The parameters studied, which might affect the extraction efficiency were extraction time, solvent composition and microwave power. The conventional heating 21 h provided 5.23 % yield of mangiferin and by microwave heating at 210 W for 56 min, the yield w...

An ionic liquids (IL)-based microwave-assisted approach for extraction and determination of flavonoids from Bauhinia championii (Benth.) Benth. was proposed for the first time. Several ILs with different cations and anions and the microwave-assisted extraction (MAE) conditions, including sample particle size, extraction time and liquid-solid ratio, were investigated. Two M 1-butyl-3-methylimid...

The fruit of Melastoma sanguineum Sims is an edible and sweet wild fruit. In our previous study, the fruit was found to have a strong antioxidant property. In this study, an ultrasound-assisted extraction (UAE) method was developed to extract natural antioxidants from the fruit of Melastoma sanguineum Sims, and a response surface methodology was used to optimize the conditions of UAE to maximiz...

A new, rapid and sensitive microextraction technique named vortex-assisted liquid-liquid-liquid microextraction (VALLLME) is proposed. The complete extraction process involves two steps. First, a vortex-assisted liquid-liquid microextraction (VALLME) procedure was used to extract the analytes from a relatively large volume of sample (donor phase) to a small volume of organic solvent (intermedia...

Rice bran is a by-product resulting from the milling process that frequently underutilized as cattle food or disposed through open-burning despite of its high nutritional and nutraceutical properties. Thus, this research aims in recognizing exploring rice extraction methods could further cultivate industry. This study focuses on using water assisted with ultrasonication. The relationship betwee...

Seaweed is a carbohydrate polymer of alginate, agar, and carrageenan which can be extracted purified as hydrocolloids. Each has different physicochemical properties hydrocolloids form gels when dispersed in water. To achieve targeted according to specific purposes functions, conventional extraction methods, several green methods for extracting seaweed have been proposed discussed. The method th...