نتایج جستجو برای: controlled crystallization
تعداد نتایج: 405292 فیلتر نتایج به سال:
taneously ND measurements we have designed a special sample holder made from insulating anodized aluminum. be accomplished considering both the primary and the secondary relaxation as being Cole-Davidson processes Upon cooling liquids may either crystallize or vitrify. Crystallization is a common phase transition by which molecules self-organize into crystals [1]. Water is one of the most impor...
In this research, crystallization of Fe36Cr12Mo10 and α-Fe phases in devitrification of Fe51Cr18Mo7B16C4Nb4 amorphous alloy was studied using X-ray diffraction and transmission electron microscopy. For evaluation of crystallization kinetics, differential scanning calorimetric tests were carried out at different heating rates. Results showed that two-step crystallization led to the formati...
Isothermal crystallization of the mono-hydroxyl alcohol n-butanol was studied with dielectric spectroscopy in real time. The crystallization was carried out using two different sample cells at 15 temperatures between 120 K and 134 K. Crystallization is characterized by a decrease of the dielectric intensity. In addition, a shift in relaxation times to shorter times was observed during the cryst...
The S-type granitoidic batholith of Shir-Kuh consists of three main granodioritic, monzogranitic and leucogranitic units. The separation of restite crystals from the primary melt, followed by the fractional crystallization, appears to have been an effective differentiation process in the batholith. Small biotite assemblages with higher XMg relative to host flaky biotites, surmicaceous enclaves,...
crystallization of aluminum fluoride at atmospheric pressure has been considered. structure, size and shape of crystals formed during the crystallization process have been investigated. by applying the direct analysis method for the existed aluminum in solution, the aluminum fluoride nucleation process has been detected as a concentration valley at the outset of crystallization process. the lin...
Saliva crystallization was previously studied in both humans and animals with various results. The study aimed to confirm of the presence of saliva crystallization in female Bornean orangutans (Pongo pygmaeus), to evaluate the quality of samples which were collected from animals and processed by keepers, and to test preliminarily if the saliva crystallization could be connected with menstrual c...
Commercial poly(p-phenylene sulfide) (PPS) was thermally cured, which resulted in an increase of molecular weight due to cross-linking. Non-isothermal crystallization studies of samples cured for up to 7 days at 250 ̊C showed a monotonous increase of crystallization temperature compared to pure PPS. However, a further increase of curing time decreased the crystallization temperature. The change ...
The crystallization behaviors of two copolymers of PVDF were studied, and the effect of copolymerized chains on the crystallization behavior was investigated. The results indicated that both copolymers had a lowered crystallization temperature and crystallinity. The crystallization rate was improved by the copolymer with symmetrical units in PVDF chains, but hindered by asymmetrical units, comp...
X-ray crystallography is the predominant method for obtaining atomic-scale information about biological macromolecules. Despite the success of the technique, obtaining well diffracting crystals still critically limits going from protein to structure. In practice, the crystallization process proceeds through knowledge-informed empiricism. Better physico-chemical understanding remains elusive bec...
In many technical applications crystallization proceeds in the presence of stresses and flows, hence the importance to understand the crystallization mechanism in simple situations. We employ molecular dynamics simulations to study the crystallization kinetics of a nearly hard sphere liquid that is weakly sheared. We demonstrate that shear flow both enhances and suppresses the crystallization k...
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