The structural stability of some nanostructured titanates was investigated in terms of their subsequent processing and possible applications. With the aim to investigate their mechanochemical stability, we applied high-energy ball milling and studied the resulting induced phase transitions. Hydrogen titanates with two different morphologies, microcrystals and nanotubes, were taken into consider...

......................................................................................................................................... ii Acknowledgements ................................................................................................................... iv List of Tables ............................................................................................................

This work outlines a systematic and detailed study of the modification anatase TiO2 with tungsten (W). The impact this coupling has on temperature to rutile phase transition photocatalytic degradation 1,4-dioxane, highly toxic compound that is increasingly present in water bodies also studied. composite photocatalysts 2, 4, 8 16 mol. % W, respectively, were produced using sol-gel process then c...

Mold powders are fluxing agents used as raw materials in the steel industry, which play very important role in processing stability and final surface quality of a product. Surface quality depends particularly on the viscosity and the heat transfer of infiltrated mold flux between the mold wall and the solidified steel shell. Heat flux across the interfacial gap depends on thermal properties of ...

We present new time-resolved powder diffraction data measured in situ during the hydrothermal crystallisation of two families of crystalline inorganic materials. In the first study, we have used time-resolved energy-dispersive X-ray diffraction (EDXRD) to follow the formation of zeolitic zinc phosphates from amine phosphates and zinc oxide in acidic solutions at 60-150 degrees C. The advantage ...

A series of supported WO3 catalysts were synthesized by incipient wetness impregnation of ammonium metatungstate aqueous solutions onto Al2O3, TiO2, Nb2O5, and ZrO2 supports as a function of tungsten oxide loading. The resulting solid acid catalysts were physically characterized with in situ Raman and UV–vis spectroscopy and chemically probed by methanol dehydration to dimethyl ether (CH3OH-TPS...

The ultrasonic-aided co-precipitation method was used to create SnO2-TiO2 nanocomposite particles. Scanning electron microscopy (SEM), X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FT-IR), and UV-vis were characterize the XRD patterns revealed crystalline structure of particles average particle size determined by Debye Scherrer’s equation found be 11.355, 4.9577, 4.333 nm fo...

Nano-crystalline TiO2 were synthesized by combustion method using metal nitrate solution and urea, glycin and citric acid fuels. Microwave irradiation was used as heating source. X-ray diffraction, scanning electron microscope as well as Fourier transform infrared spectroscopy were performed to characterize the obtained samples. X-ray diffraction patterns revealed that in the case of citric aci...