in this paper, plate-like nio nanoparticles were prepared by one-pot solid-state thermal decomposition of nickel (ii) schiff base complex as new precursor. first, the nickel (ii) schiff base precursor was prepared by solid-state grinding using nickel (ii) nitrate hexahydrate, ni(no3)2∙6h2o, and the schiff base ligand n,n′-bis-(salicylidene) benzene-1,4-diamine) for 30 min without using any solv...

In the present study, ZnO nanostructure has been synthesized by different methods, namely coprecipitation, hydrothermal and sonochemical methods. After comparison of the morphology and photocatalytic activity of ZnO samples prepared via different methods, the best method (sonochemical method) was used for synthesis of Ni-ZnO nanoparticles with different concentrations of nickel. Furthermore, st...

in this work, copper oxide nanoparticles have been synthesized via extractive rosmarinus officinalis leaves by simple and economic co-precipitation method at ambient conditions which it has used (ch3coo)2cu+h2o individually as cu sources. it was found that uniform copper oxide nanoparticles have been successfully produced at various temperature, namely 400, 600, and 800 0c. powder x-ray diffrac...

in this paper, cubic nickel oxide nanoparticles were successfully prepared by solid-state thermal decomposition of nickel(ii) macrocyclic schiff-base complex at 450°c for 3 h without employing toxic solvent or surfactant and complicated equipment. nickel(ii) macrocyclic schiff-base complex was synthesized by the reaction of 1,2-bis(2-formyl-3-methoxyphenyl)propane, nicl2•6h2o and 1,3-phenylened...

Considering the wide range of applications of metal–polymer composites, composite of Fe-polyimide has been obtained by plasma sputtering method, also polyimide films were treated with plasma. Comparative study of surface modification of the composite film and the polyimide film due to Fe doping and plasma treatment have been studied, using the contact angle measurement, scanning electron micros...

the objective of the present study is to develop and investigate the swelling behavior of ph-sensitive superporous hydrogel (sph) and sph composite (sphc). a novel superporous hydrogel containing poly (methacrylic acid-co-acrylamide) was synthesized from methacrylic acid and acrylamide through the aqueous solution polymerization, using n,n-methylenebisacrylamide as a crosslinker and ammonium pe...

the synthesis, characterization and application of biologically synthesized nanomaterials are an important aspect in nanotechnology. the present study deals with the synthesis of silver nanoparticles (ag-nps) using the aqueous extract of red seaweed gelidiella acerosa as the reducing agent to study the antifungal activity. the formation of ag-nps was confirmed by uv-visible spectroscopy, x-ray ...

zinc oxide nanotubes were prepared by a hydrothermal method using zinc nitrate as a precursor. The synthesized nanotubes were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), Transmission electron microscopy (TEM), Fourier transform infrared spectroscopy (FT-IR) and their optical properties were characterized using UV -visible spectroscopy. The XRD analysis confirme...

The zinc-cadmium oxide (ZnO-CdO) nanocomposites with different weight percentages of cadmium oxide (CdO) nanoparticles were successfully synthesized by the sonochemical method using zinc and cadmium nitrates as precursors to probe their nano-structured surfaces for the decomposition reactions of chloroethyl phenyl sulfide (CEPS) as a surrogate of sulfur mustard agent simulant. Scanning electron...

Nanolayered Mn oxide/poly(4-vinylpyridine) as a model for Mn cluster in photosystem II was synthesized and characterized using scanning electron microscopy (SEM), transmission electron microscopy (TEM), dynamic light scattering (DLS), Fourier transform infrared spectroscopy (FTIR) and UV-Visible spectroscopy (UV-Vis). The compound is a very efficient water oxidizing catalyst, and sizable oxygen...