Ionic liquid 1-butyl-3-methylimidazolium bromide-methanol-based ultrasonic-assisted extraction (ILUAE) was used to extract tilianin and acacetin from the aerial parts of Agastache rugose (A. rugose), and simultaneously determined by reversed phase high performance liquid chromatographic (RP-HPLC) method with ultraviolet detection (RP-HPLC-UV). An InertSustain RP-C18 column was used with the mob...

A commercial pharmaceutical analysis chiral method development kit (Chirex Column Kit A, Phenomenex) was used to analyze six pesticide stereoisomer mixtures. The pesticides were selected from the 1994-1995 National Water Quality Assessment Program (NAWQA) covering New Mexico and Texas. Three stereoisomer mixtures were separable on three different columns. The instrumental detection limit and de...

Liquid-liquid extraction and solid phase followed by high-performance liquid chromatography (HPLC) connected with ultraviolet (UV) detection were used for the determination of phytohormones. The parameters influencing performance HPLC-UV method, including composition mobile gradient elution, column temperature, flow rate, wavelength, optimized. This method can simultaneously determine 11 phytoh...

The effects and influences of various operational parameters on the efficiency of mixer-settlers are thoroughly studied in this paper. One of the most important factors in designing a mixer-settler is to obtain an optimum operational extraction and overall efficiency. These two factors are dependent on various parameters such as impeller shape, size and speed of impeller, baffle size, residence...

Ochratoxin A (OTA) is a widespread and abundant natural carcinogenic mycotoxin produced by several species of Aspergillus and Penicillium fungi. Due to the ubiquitous presence of these fungi in food and potential risk for human health, a rapid and sensitive in vitro detection assay is required. Analytical methods for OTA detection/identification are generally based on liquid-liquid extraction, ...

Spectrometric techniques for the analysis of trace cadmium have developed rapidly due to the increasing need for accurate measurements at extremely low levels of this element in diverse matrices. This review covers separation and preconcentration procedures, such as electrochemical deposition, precipitation, coprecipitation, solid phase extraction, liquid-liquid extraction (LLE) and cloud point...

Here we report on the development of a selective and sensitive high-performance liquid chromatographic method for the determination of lidocaine in human serum. The extraction of lidocaine and procainamide (internal standard) from serum (0.25 mL) was achieved using diethyl ether under alkaline conditions. After liquid-liquid extraction, the separation of analytes was accomplished using reverse ...

Venlafaxine (VEN), which was introduced into the therapy in 1990s, is one of the most often used antidepressants. The monitoring of its level in the human organism is recommended, particularly in the case of a patient suffering from other illnesses and treated with different drug substances interfering with VEN. The most popular diagnostic material for the quantitation of VEN is blood. The pres...