This review aims at summarizing the most recent updates in the field of acrylamide (AA) formation (mechanism, conditions) and the determination of AA in a number of foods (fried or baked potatoes, chips, coffee, bread, etc). The methods applied for AA detection [Capillary Electrophoresis-Mass Spectrometry (CE-MS), Liquid Chromatography-Mass Spectrometry (LC-MS), Non-Aqueous Capillary Electropho...

Ionic liquid-based dispersive liquid–liquid microextraction (IL– –DLLME) coupled with high performance liquid chromatography (HPLC) with UV detection was developed for the simultaneous extraction and determination of nickel, cobalt, copper and zinc ions. In the proposed approach, salophen (N,N'-bis(salicylidene)-1,2-phenylenediamine) was used as a chelating agent, the ionic liquid, 1-hexyl-3-me...

A new radioanalytical method was developed for rapid determination of (226)Ra in human urine samples. The method is based on organic removal and decolourisation of a urine sample by a polymeric (acrylic ester) solid phase sorbent material followed by extraction and preconcentration of (226)Ra in an organic solvent using a dispersive liquid-liquid microextraction technique. Radiometric measureme...

abstract polycyclic aromatic hydrocarbons (pahs) are classified as persistent and carcinogenic organic pollutants. pahs contamination has been reported in water. many of relevant regulatory bodies such as eu and epa have regulated the limit levels for pahs in drinking water. in this study, 13 priority polycyclic aromatic hydrocarbons (pahs) were determined in tap water samples of tehran and wat...

AbstractThe oldest method for the managing of the illness is the use of medicinal plants. The use of herbal products as the first choice in self-treatment of minor conditions continues to expand rapidly across Iran. This makes the safety of herbal products an important public health issue.Pesticides are used widely in agriculture to increase the production by controlling the harmful insects and...

This paper describes a new approach for the determination of amitriptyline in wastewater by ionic liquid based immersed droplet microextraction (IL-IDME) prior to high-performance liquid chromatography with ultraviolet detection. 1-Hexyl-3-methylimidazolium hexafluorophosphate ([C6MIM][PF6]) was used as an ionic liquid. Various factors that affect extraction, such as volume of ionic liquid, sti...

an air–assisted liquid–liquid microextraction method for the extraction and preconcentration of trace amounts of some synthetic phenolic antioxidants in biological fluids followed by their determination by gas chromatography–flame ionization detection has been reported. in this method the target analytes are extracted into a few microliters of carbon tetrachloride (extraction solvent) from an a...

dispersive liquid liquid microextraction (dllme) combined with gas chromatography–mass spectrometry (gc–ms) was used for the extraction and determination of 13 polycyclic aromatic hydrocarbons (pahs) in mineral water samples. in this procedure, the suitable combination of extraction solvent (500 µl chloroform) and disperser solvent (1000 µl acetone) were quickly injected into the water sample (...