A method for the simultaneous determination of the colorants Sunset Yellow FCF and Quinoline Yellow using solid-phase spectrophotometry is proposed. The colorants were isolated in Sephadex DEAE A-25 gel at pH 5.0, the gel-colorants system was packed in a 1 mm silica cell and spectra were recorded between 400 and 600 nm against a blank. Statistical results were obtained by partial least squares ...

Definitions of the concepts of bias and recovery are discussed and approaches to dealing with them described. The Guide To Uncertainty in Measurement (GUM) recommends correction for all significant systematic effects, but it is also possible to expand measurement uncertainty to take account of uncorrected bias. Run, laboratory and method bias can be defined as components of the bias of a partic...

Based on the analysis of known methods technical solutions, a two-stage method calibration receiving active phased array antenna (AFAR) long-range detection radar station (RLS) is proposed. The peculiarity this algorithm, which does not require physical modification and use expensive measuring equipment, makes it possible to determine difference in characteristics AR channels compensate for dif...

the application of a flight simulator with six degree of freedom (6dof)) in design and analysis of rocket systems is essential. the calibration of a 6dof flight simulator is a challenging problem. this paper focuses on the calibration of a flight simulator and intends to answer the following questions: 1) does experimental design have significant impact on calibration quality? if so, which expe...

OBJECTIVES Our aim was to improve meta-analysis methods for summarizing a prediction model's performance when individual participant data are available from multiple studies for external validation. STUDY DESIGN AND SETTING We suggest multivariate meta-analysis for jointly synthesizing calibration and discrimination performance, while accounting for their correlation. The approach estimates a...

iron, cobalt and copper are metals, which appear together in many real samples, both natural and artificial. recently a classical univariate micellar colorimetric method has been developed for determination of these metal ions. the organized molecular assemblies such as micelles are used in spectroscopic measurements due to their possible effects on the systems of interest. the ability of micel...

The predictability of multivariate calibration models, calculated with offline near-infrared spectroscopy (NIRS), assessing impact of magnesium stearate (MgSt) fraction, blending time, and compression force on the tablet breaking force (TBF) of SPRESS® B820 was statistically compared. Tablets of lubricated SPRESS® B820 were prepared by varying lubrication and compression conditions using 24 ful...

FTIR spectroscopy in combination with multivariate calibrations, i.e. partial least square (PLS) and principle component regression (PCR) was developed for quantitative analysis of cod liver oil (CLO) in binary mixture with corn oil (CO). The spectra of CLO, CO and their blends with certain concentrations were scanned using horizontal attenuated total reflectance (HATR) accessory at mid infrare...

The mathematical model of Area-Reduction empirical method is written through MATLAB software. Three periods of the hydrologic survey are required to run, calibrate and validatethe model. The Dez Dam, which is one of the most significant dams of the Middle East with three periods of hydrographic surveys in 1972, 2002 and 2011, has been chosen for the investigation. The annual average of the inpu...