In this work, we present a novel method for the synthesis of copper nanoparticles. We utilize the charge compensatory effect of ionic liquid [bmim]BF(4) in conjunction with ethylene glycol for providing electro-steric stabilization to copper nanoparticles prepared from copper sulphate using hydrazine hydrate as a reducing agent. The formed copper nanoparticles showed extended stability over a p...

Charged-coupled device (CCD) detectors have been widely accepted as detectors for collecting X-ray diffraction images. The CCD detector offers a sensitive detection system well suited for diffraction analysis and, compared with other detectors on the market, a relatively rapid system for read-out of the collected image. The two predominant markets for the CCD detector have been those in which r...

Nickel films of 300 nm thickness were deposited by electron beam evaporation at room temperature on 316 stainless steels. Corrosion studies of Ni coated 316 SS have been performed after N+ ion implantation at different energies of 20, 40, 60 and 80 keV. The structure and surface morphology of the films were evaluated using X-ray diffraction (XRD), atomic force microscope (AFM) an...

Here, we report the synthesis, characterization, and catalytic evaluation of Ni-Cu-Mg ferrite using tragacanth gum as biotemplate and Metals nitrate as the metal source by the sol-gel method without using any organic chemicals. The sample was characterized by powder X-Ray Diffraction (XRD), Fourier Transform Infrared Spectroscopy (FT-IR), Vibrating Sample Magnetometer (VSM), and Scanning El...

In this study, we have reported the green synthesis magnesium ferrite using tragacanth gel by the sol-gel method without using any organic chemicals. The sample was characterized by powder X-ray diffraction (XRD), Fourier Transform Infrared Spectroscopy (FTIR), vibrating sample magnetometer (VSM) and scanning electron microscopy (SEM). The X-ray powder diffraction (XRD) analysis revealed the fo...

ZnS  nanoparticles  were  synthesized  via  a  simple  surfactant  free microwave  route.  In  this  synthesis, thioacetamide  was  used  as sulfur  source.  The effects  of different  parameters  such  as  type of zinc precursor,  time  and  power  of  irradiation  on  the  morphology and  particle  size  of  the  products  have been  investigated.  The nanostructures  were  characterized  by ...

cuins2 nanostructures were  synthesized  via  a  simple  surfactant-free solvothermal  route.  in  this  synthesis,  thiosemicarbazide  and thioglycolic acid were used as sulfur sources. the effects of different parameters such as type of precursor and time on the morphology and particle  size  of  the  samples  have  been  investigated.  the nanostructures  were  characterized  by  means  of  ...