نتایج جستجو برای: ray diffraction and ftir

تعداد نتایج: 16884555  

Journal: Nanomedicine Journal 2016

Objective(s): Chitosan nanoparticles (CNPs) were prepared based on the ionic gelation of chitoan with anionic compounds of Ocimum basilicum leaf extract. Materials and Methods: After addition of Ocimum basilicum leaf extract to chitosan solution, the physicochemical properties of the nanoparticles were determined by Field Emission Scanning Electron microscope (FESEM), Fourier Transform Infrared...

2012
K. Selvaraju S. Kumararaman

A new semi-organic nonlinear optical thiosemicarbazide cadmium acetate (TSCA) material has been synthesized. TSCA single crystals were grown from aqueous solution by slow evaporation method. The solubility of TSCA has been determined for various temperatures. The grown crystals were characterized by single crystal X-ray diffraction (XRD), FTIR, UV-Vis., thermal and second harmonic generation (S...

Journal: :علوم و تکنولوژی پلیمر 0
مهدی نکومنش حسن عربی غلامرضا نجابت مهرسا امامی غلامحسین ظهوری

mcm-41 is one of the groups of mesoporous materials that have wide applications as adsorbents, ion exchangers and catalyst supports. in this work spherical and rod-like mcm-41s were synthesized in homogeneous and heterogeneous reaction media, respectively. for synthesis of these materials the cationic surfactant cetyltrimethylammonium bromide (ctmabr) was used as template and tetraethylorthosil...

Journal: :The journal of physical chemistry letters 2017
Pan Wang Jiwen Guan Draven T K Galeschuk Yansun Yao Cindy F He Shan Jiang Sijia Zhang Ying Liu Meiling Jin Changqing Jin Yang Song

Formamidinium lead iodide (FAPbI3) perovskite as a superior solar cell material was investigated in two polymorphs at high pressures using in situ synchrotron X-ray diffraction, FTIR spectroscopy, photoluminescence (PL) spectroscopy, electrical conductivity (EC) measurements, and ab initio calculations. We identified two new structures (i.e., Imm2 and Immm) for α-FAPbI3 but only a structural di...

Journal: :Molecules 2016
Dan Wei Lixin Chen Tingting Xu Weiqi He Yi Wang

A preceramic polymer of B,B',B''-(dimethyl)ethyl-acrylate-silyloxyethyl-borazine was synthesized by three steps from a molecular single-source precursor and characterized by Fourier transform infrared (FTIR) and nuclear magnetic resonance (NMR) spectrometry. Six-member borazine rings and acrylate groups were effectively introduced into the preceramic polymer to activate UV photo-induced polymer...

اسمعیلی, لیلا , قلی‌زاده, احمد ,

In this research, the effect of temperature and concentration of bismuth nitrate mole on structural, magnetic and photocatalytic properties of the bismuth ferrite nanoparticles prepared by nitrate-citrate method have been investigated. The structural and magnetic properties were characterized by X-ray diffraction (XRD), Fourier-transform infrared spectroscopy (FTIR) and vibrating-sample magneto...

Journal: :journal of sciences, islamic republic of iran 2011
r. sepahvand

in the present work, magnetic nanocomposites of the multi-walled carbon nanotubes (mwcnts) decorated with magnesium ferrite (mgfe2o4) nanoparticles were synthesized successfully by citrate-gel method. the shape, structure, size, and properties of the as-synthesized sample were characterized by fourier transform infrared spectroscopy (ftir), x-ray diffraction pattern (xrd), transmission electron...

Journal: :Physical chemistry chemical physics : PCCP 2012
René Moré Mirko Scholz Gehard Busse Lennart Busse Carsten Paulmann Martin Tolkiehn Simone Techert

We compare results from single crystal X-ray diffraction and FTIR spectroscopy to elucidate the nature of hydrogen bonding in β-9-anthracene carboxylic acid (β-9AC, C(15)H(10)O(2)). The crystallographic studies indicate a disorder for the protons in the cyclic hydrogen bond. This disorder allows the determination of the energy difference between two proton sites along the hydrogen bond. The tem...

2014
David M Pickup Robert J Newport Emma R Barney Ji-Yung Kim Sabeel P Valappil Jonathan C Knowles

In this study, amorphous (Na2O)x(CaO)0.50- x(P2O5)0.50·yH2O (where x = ~0.15 and y = ~3) samples were prepared by a coacervate method. Thermal analysis showed that two types of water molecules were present in the coacervate structures: one type loosely bound and the other part of the phosphate structure. Structural studies using Fourier transform infrared spectroscopy (FTIR) and X-ray total dif...

F. Barikan S. Khanahmadzadeh,

Polyimide/Nickel oxide (polyimide/NiO) nanocomposite was successfully synthesized by sol gel technique, using Pyromellitic dianhydriede (PMDA), 4,4-oxydianiline (ODA) and N,N-dimethylacetamide (DMAC) and 10 wt% Nickel titanate nanopowders (NPs). Fourier transform infrared spectrometry (FTIR), X-ray diffraction (XRD), scanning electron microscopy (SEM), and vibrating sample magnetometer (VSM) we...

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