In this research, FeNi@PANI nanocomposites as the electromagnetic wave absorbers were prepared through two following steps. At first, FeNi alloy nanoparticles were synthesized by the one-pot polyol process, and then, in-situ polymerization method was used for the preparation of FeNi@PANI nanocomposite. The XRD pattern confirmed the formation of pure FeNi alloy with the FCC crystalline phase. Th...