dispersive liquid–liquid micro–extraction (dllme) technique was successfully used as a sample preparation method for the determination of clonazepam in pharmaceutical preparations and water samples. in this method, a suitable mixture of methanol (disperser solvent) and chloroform (extraction solvent) was injected rapidly into a conical test tube that contained an aqueous solution of clonazepam....

The separation of Rare Earth Elements (REEs) is an important step in the valorization REE ore and aims at producing individual rare earth compounds for market. carried out industrially by solvent extraction (SX) using interconnected circuits consisting cascades mixer-settlers. design a circuit implies selection operating conditions number mixer-settlers required to achieve target degree purity ...

The ability of a solute (inorganic or organic) to distribute itself between an aqueous solution and an immiscible organic solvent has long been applied to separation and purification of solutes either by extraction into the organic phase, leaving undesirable substances in the aqueous phase; or by extraction of the undesirable substances into the organic phase, leaving the desirable solute in th...

Research into the solvent extraction of iron(III) from a chloride solution after bauxite HCl leaching by neutral oxygen-containing extractants and their mixtures were studied degree solutions using alcohols is presented. The effect dilution alcohol with ketone an mixture in relation to its effectiveness was investigated. efficiently extracted 1-octanol 1-decanol (70%) 2-undecanone (30%) hydroch...

Gloriosa superba is a medicinal plant used in traditional medicine for the treatment of various diseases. The tuber of Gloriosa superba is a rich source of colchicine which is used for the treatment of gout, cirrhosis and also used in plant breeding studies to produce polyploidy. Optimization of various extraction parameters using response surface methodology (RSM) was performed to assess maxim...

A sensitive determination method was developed for the analysis of pyrethroid pesticide residues in tomato samples using ionic liquid-based dispersive liquid-liquid microextraction. A hydrophobic ionic liquid (1-butyl-3-methylimidazolium hexafluorophosphate) and acetonitrile were used as the extraction solvent and dispersive solvent, respectively. The following experimental parameters affecting...

Solvent extraction is the most widely used method for separation and purification of rare earth elements, organic extractants such as di(2-ethylhexyl) phosphoric acid (P204) di(1-methyl-heptyl) methyl phosphonate (P350) are commonly industrial applications. However, presence impurity ions in feed liquid during can easily emulsify extractant affect quality products. Aluminum ion common liquid, i...

Beyond hydrogen storage: The first example of reversible magnesium deposition/stripping onto/from an inorganic salt was seen for a magnesium borohydride electrolyte. High coulombic efficiency of up to 94 % was achieved in dimethoxyethane solvent. This Mg(BH(4))(2) electrolyte was utilized in a rechargeable magnesium battery.

The effects of different solvents, temperature conditions, solvent-solid ratios and particle sizes on solid-solvent extraction of the total phenolics, proanthocyanidins and flavonoids herein also referred to as antioxidant from pomegranate marc peel (PMP) was studied. Water, methanol, ethanol, acetone, and ethyl acetate extraction efficiencies at extraction times of 0.17 to 10 min, extraction t...