نتایج جستجو برای: solvent free microwave extraction

تعداد نتایج: 758549  

2012
Chunhui Ma Lei Yang Wenjie Wang Fengjian Yang Chunjian Zhao Yuangang Zu

An ultrasound and microwave assisted alternant extraction method (UMAE) was applied for extracting dihydroquercetin (DHQ) from Larix gmelinii wood. This investigation was conducted using 60% ethanol as solvent, 1:12 solid to liquid ratio, and 3 h soaking time. The optimum treatment time was ultrasound 40 min, microwave 20 min, respectively, and the extraction was performed once. Under the optim...

2017
Fernanda Carolina Sousa Fonseca Letícia Caribé Batista Reis Jener David Gonçalves dos Santos Carla Rodrigues Cardoso Branco Sergio Luis da Costa Ferreira Jorge Mauricio David Alexsandro Branco

BACKGROUND The effect of the extraction time (min) and temperature (°C) on the yield of betulinic acid (BA) from Zizyphus joazeiro barks using focused microwave-assisted extraction was investigated. MATERIALS AND METHODS The ethyl acetate was used as extractor solvent because it was shown to provide a betulinic acid-clean extract. A full two-level statistical factorial design was applied to d...

2003
Judith R. Denery Klaus Dragull C. S. Tang Qing X. Li

Pressurized fluid extraction (PFE) was examined as an alternative technology for the extraction of carotenoids in the green algae Haematococcus pluvialis and Dunaliella salina and kavalactones in Piper methysticum. The extraction process was optimized by varying the key extraction factors of solvent, sample-solvent ratio, temperature, and time. The selectivity and efficiency of extraction param...

Journal: :Bulletin of the Korean Chemical Society 2013

Journal: :Biomedical chromatography : BMC 2012
Ting Zhou Xiao-Hua Xiao Jia-Yue Wang Jin-Ling Chen Xian-Fang Xu Zhi-Feng He Gong-Ke Li

In this paper, a microwave-assisted extraction (MAE) method was established for aristolochic acid-I from Aristolochiae Fructus, and the advantage of MAE was evaluated by chromatographic analysis coupled with nephrotoxicity studies. The experimental parameters of MAE for aristolochic acid-I in Aristolochiae Fructus were investigated and MAE was compared with Soxhlet extraction and ultrasound-ass...

2006
D. Bera D. Lahiri A. De Leonardis Antonella De Leonardis A. Nag

Hexane, the common solvent for extraction of edible oils from seeds is no more considered safe due to the presence of solvent in oil and also solvent vapour, a hazardous air pollutant. We have carried out the experiments with bahera (Terminalia bellerica Roxb) and flax seed (Linum usitatissimum ) oil as these oils are highly used in food for their nutraceutical values. The extraction of edible ...

Journal: :organic chemistry research 2016
arezoo pourkazemi abdolkarim zare

in this research, so3h-functionalizedphthalimide (sfp) has been prepared through simple reaction of phthalimide with chlorosulfonic acid, and characterized using ft-ir, 1h nmr, 13c nmr, sem (scanning electron microscopy), mass and tg (thermal gravimetric) spectra. afterward, the solid acid has been utilized as an efficient, green, heterogeneous and recyclable catalyst for the solvent-free synth...

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