نتایج جستجو برای: thermogravimetry analysis
تعداد نتایج: 2824606 فیلتر نتایج به سال:
In this work, the relationship between cellulose crystallinity, the influence of extractive content on lignocellulosic fiber degradation, the correlation between chemical composition and the physical properties of ten types of natural fibers were investigated by FTIR spectroscopy, X-ray diffraction and thermogravimetry techniques. The results showed that higher extractive contents associated wi...
carbon nanotubes were synthesized over a series of zn-containing fe/alumina catalysts by chemical vapor deposition method at two reaction temperatures of 850 and 950 °c using methane as a carbon source. catalysts were synthesized by keeping fe concentration constant and varying zn concentration to study the effects of zn. the catalysts were characterized using x – ray powder diffraction and n2 ...
Polyvinyl alcohol (PVA) / starch (S) /Carboxy methyl cellulose (CMC) / Montmorillonite (MMT) bionanocomposite films were prepared from PVA, MMT, CMC and soluble starch aqueous suspensions by casting method in the presence of a plasticizer that contained glycerol. The kinetics of thermal degradation of PVA/S/CMC/MMT blends was investigated by thermogravimetry (TGA) and derivative thermogravimetr...
A quantitative evaluation of wood chemical components for some tree species in a forest area from east-northern Romania is presented here, through a comparative study from 1964 to 2000. Investigation upon the wood tree-rings in a Quercus robur L. tree species, as a dominant species, as regards its chemical composition and structure of the natural polymer constituents cellulose and lignin was al...
The evaluation of compost stability is of the utmost importance for the reliability of composting as a recycling strategy. To date there is no single parameter that can give a sure indication of the stability of composts from different starting materials. This paper investigates different methods of evaluating the dynamics of transformation of materials and the stability level of the end produc...
Superhydrophobic surfaces are attractive as self-cleaning protective coatings in harsh environments with extreme temperatures and pH levels. Hexagonal phase boron nitride (h-BN) films are promising protective coatings due to their extraordinary chemical and thermal stability. However, their high surface energy makes them hydrophilic and thus not applicable as water repelling coatings. Our recen...
A novel nanocomposite based on poly(N-octadecyl-2-ethynylpyridinium bromide) (PNOEtPyBr) and Mg(0.04)Nb(1.66)O5 nanosheets is synthesized by the method of exfoliation-reflocculation. The XRD data of the nanocomposite indicates the formation of Mg(0.04)Nb(1.66)O5 nanosheets/PNOEtPyBr nanostructure with an interlayer expansion of 4.6 nm along a direction perpendicular to the Mg(0.04)Nb(1.66)O5 na...
Abstract In the present work, PLA-PBS blends of 80/20 weight ratio were doped with zinc oxide (2.5; 5; 7.5 and 10 phr) flow, thermogravimetric thermomechanical behaviour resulting investigated. Using capillary plasstometry, thermogravimetry (TGA) dynamic mechanical analysis (DMA), it was found that increase in content resulted an flow indices (MFI, MVR), as well storage loss modulus values, a d...
[60]Fullerene hexakisadducts possessing 12 carboxylic acid side chains form crystalline hydrogen-bonding frameworks in the solid state. Depending on the length of the linker between the reactive sites and the malonate units, the distance of the [60]fullerene nodes and thereby the spacing of the frameworks can be controlled and for the most elongated derivative, continuous channels are obtained ...
Polyvinyltetrazole (PVT) is produced from acrylonitrile (AN) monomer by using free-radicalpolymerization and Click Chemistry methods. The resulting polymer with a broad range of tetrazolegroup contents was conveniently synthesized through [3+ 2] azide-nitrile cycloaddition reaction ofnitrile-containing polymer with sodium azide in DMF. The prepared PVT was characterized by13CN...
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