Fritillaria is a traditional Chinese herbal medicine for anti-tussive and expectorant use in China and some other Asian countries. The Fritillaria Chinese medicine material derived from different geographical origins is always difficult to discriminate each other. The objective of the study is to develop a nondestructive and simple method to identify five Fritillaria Chinese materia medica such...

A high-precision diffractometer has been developed for the structure analysis of a submicrometre-scale single grain of a powder sample at the SPring-8 BL40XU undulator beamline. The key design concept is the combination of a stable focused synchrotron radiation beam and the precise axis control of the diffractometer, which allows accurate diffraction intensity data of a submicrometre-scale sing...

In the present study, nanocrystalline Ni50Al50-xMox (X = 0, 0.5, 1, 2.5, 5) intermetallic compound was produced through mechanical alloying of nickel, aluminum, and molybdenum powders. AlNi compounds with good and attractive properties such as high melting point, high strength to weight ratio and high corrosion resistance especially at high temperatures have attracted the attention of many rese...

BACKGROUND The Fourier space (reciprocal space) image of bulk polyethylene consists of lines superimposed on the coherent diffuse background. The mixed character of the image indicates the complex nature of these compounds. The inability in detecting full images of reciprocal space of polymeric substances without Compton radiation and the other undesirable diffuse scatterings has misled the str...

carbonates are among the most common soil constituents in arid and semiarid zones. they exhibit many significant differences in their chemical and mineralogical, suite, origin, physical and micromorphological properties and consequently in their activities in soil. the differences cause different properties of calcareous soils. six profiles of aridisols and inceptisols with carbonate accumulati...

spherical granules of the superionic conductor β/β́ lizr2(po4)3 in the range of sub 100 nm sizewere synthesizedvia freeze drying methodand fully reviewed in all aspects. samples were characterized by the x-ray diffractometry (xrd), the thermal analysis (tg, dsc), thefourier transform infra-red spectroscopy (ftir) and the scanning electron microscopy (sem).their structuredepends largely on the me...

      Glipizide has been found to form inclusion complexes with β-cyclodextrin (β-CD) in solution and in solid state. The present study was undertaken to determine a suitable method for scaling up glipizide-β-CD inclusion complex formation and to evaluate the effect of some parameters on the efficiency of complexation. The solid inclusion complexes of glipizide and β-CD were prepared at a molar...

Characterization of clarithromycin polymorph was performed by solid-state cross polarization and magic angle spinning (CP/MAS) 13C-NMR spectroscopy. Two polymorphs, form II and form I, of clarithromycins indicated characteristic resonances of C1 carbonyl carbon at 176.2 and 175.2 ppm, respectively. Since each peak of C1 carbon was well separated in the spectrum of the two polymorphs, we perform...

this article presents the method of extraction-preconcentration of lead, cadmium, and nickel ions from food samples using the ghezeljeh montmorillonite nanoclay (geleh-sar-shoor) as a new native adsorbent in batch single component systems. the extraction-preconcentration of heavy metals were carried out by applying the solid phase extraction (spe) method followed by atomic absorption spectrosco...

colloidal nanosilica is currently being produced by various methods which are mainly high energy intensive and/or not environmentally friendly. it is therefore essential to develop new energy-efficient and environmentally friendly technologies. this paper introduces a new ultrasound assisted route based on alkali leaching of silica fume for synthesis of colloidal silica nanoparticles. the ef...