Amorphous and crystalline powder of PLT phase was synthesized by using the Pechini method. Infrared (FTIR) analysis of the polymeric resin shows intense bands of organic materials from 250 to 1620 cm−1. X-ray diffraction (XRD) and Raman spectra of calcined powder at different temperatures show amorphous phase at 450 ◦C/3 h, semi-crystalline phase at 550 ◦C/3 h and a crystalline phase at 800 ◦C/...

tio2 nanorods can be used as dye-sensitized solar cells and as various sensors and photocatalysts. these nanorods are synthesized by a using thermal corrosion process in a naoh solution at 200 oc with tio2 powder as a source material. in the present work, the synthesis of tio2 nanorods in anatase, rutile and ti8o15 phases and the synthesis of tio2 nanorods by using the sol-gel method and alkali...

in this paper cufe2o4, nanocrystalline powders were prepared. also, the supported cu ferrite was obtained by impregnation of the supports with cu and fe nitrates solutions, for calcination temperature 450 ºc. the samples were characterized by x-ray powder diffraction (xrd) and fourier transform-infrared spectroscopy (ft-ir). in this investigation photocatalytic degradation of acid red 206 in wa...

High crystallinity of ZnWO4 nanoparticles has been successfully synthesized via a highly effective and environmentally friendly microwave route by controlling the reaction time and temperature. The products were characterized by X-ray powder diffraction (XRD), transmission electron microscopy (TEM), and Fourier infrared spectrum (FT-IR). The crystallinity was enhanced with the increase of the r...

A bifunctional nanocatalyst composed of iron containing SBA-15 material modified with sulfonic acid groups was synthesized by a mechanochemical approach. A full characterization of the obtained nanocatalyst was performed by N2 physisorption isotherms analysis, transmission electron microscopy (TEM), X-ray powder diffraction (XRD) and Fourier-Infrared Spectroscopy (FT-IR). The mechanochemically ...

A comparative study of two coating methods on titanium (Ti) substrates, sol-gel and electrophoresis processes, was performed. Before coating, two different surface treatments were employed. The hydroxyapatite (HA) powder were characterized by infrared spectroscopy (FTIR) and X-ray diffraction (XRD) while coated samples were examined by using scanning electron microscopy (SEM) with energy disper...

The silk yarn containing Ag nanoparticles was prepared through the chemical reduction under ultrasound irradiation. In this system, ethylene glycol served as a reduction reagent and protecting silver nanoparticles from aggregation. The effect of some parameter, such as power of ultrasound irradiation and temperature in growth of the nanometric Ag were studied. Particle sizes and morphology of n...

The mechanochemical dechlorination of pentachlorophenol (PCP) was studied using CaO and SiO2 powder as additives. The effects of the milling time and additives on the dechlorination rate were investigated. The resulting product was characterized by X-ray diffraction (XRD), Fourier transform infrared spectra (FT-IR), thermogravimetric analysis (TG) and ion chromatography (IC). It is found that g...

Spherical microparticles, capable of responding to magnetic fields, were prepared by encapsulating dextran-coated Fe3O4 nanoparticles into chitosan poly(acrylic acid) (PAA) microspheres template. The obtained magnetic microspheres were characterized by transmission electron microscopy (TEM), Fourier transform infrared spectroscopy (FT-IR), scanning electron microscopy (SEM), X-ray powder diffra...

The catalyst containing 80%Co/20%Ce/15wt%SiO2 was prepared using fusion procedure and studied for the conversion of synthesis gas to light olefins. The effect of a range of operating variables such as the pressure, temperature and H2/CO molar feed ratio on the catalytic performance of fused catalyst was investigated. It was found that the best operating conditions are H2/CO=2/1, T=350 ̊C and P=2...