A filter based on the Hankel Lanczos Singular Value Decomposition (HLSVD) technique is presented and applied for the first time to X-ray diffraction (XRD) data. Synthetic and real powder XRD intensity profiles of nanocrystals are used to study the filter performances with different noise levels. Results show the robustness of the HLSVD filter and its capability to extract easily and efficiently...

Nano size nickel copper ferrite powders (NiCuFe2O4) have been prepared by a prepared by Co precipitation method. The resulting powders were characterized by X-ray diffraction (XRD), Scanning electron microscope (SEM).The result showed nanosize nickel copper ferrite(35.65nm). The powders showed extensive XRD line broadening and sizes of crystals observed from the XRD line broadening was35.65 nm,...

The aim of the presented research was to analyze ceramic material based on cordierite as a function activation time and sintering temperature. Three-component oxide mixture prepared (MgO + Al2O3 SiO2 in ratio 2:2:5). To decrease temperature, 10 mass % Bi2O3 added this mixture. mixtures were mechanically activated for 5 240 minutes ball mill. Activated sintered at temperatures 1173-1573K. XRD me...

Synchrotrons can be used to generate X-rays in order to probe materials at the atomic level. One approach is to use X-ray diffraction (XRD) to do this. The data from an XRD experiment consists of a sequence of digital image files which for a single scan could consist of hundreds or even thousands of digital images. Existing analysis software processes these images individually sequentially and ...