Several elements (V, Mo, Fe, Mn, Cd, Zn) as metallic impurities in pure uranium compounds were quantitatively determined by atomic absorption spectrometry. The effects of uranium and that of other factors on the absorption intensity of each element were studied. The analyzed samples were dissolved in 6 M nitric acid, and uranium was selectively extracted with tributylphosphate. The aqueous solu...

In the present study seven synthetic polymers were used as adsorbents for the removal of Cd(II) from aqueous solution. The equilibrium studies were systematically carried out in a batch process, covering various process parameters that include agitation time, adsorbent dosage, and pH of the aqueous solution. The analyzing system was an atomic absorption spectrometer (Perkin-Analyst 100). It was...

background: nickel is an important constituents widely used in different industrial processes for production of various syn¬thetic materials. for evaluation of workers’ exposure to trace toxic metal of ni (ii), environmental and biological monitor¬ing are essential processes, in which, preparation of samples is one of the most time-consuming and error-prone as¬pects prior to analysis. methods: ...

We describe an inductively coupled plasma atomic emission spectrometer that has been adapted to perform routine, simultaneous, direct analyses of calcium, magnesium, copper, zinc, and iron in serum or urine without sample digestion or pretreatment. The system, constructed with inexpensive, readily available components, can analyze 1-mL or smaller samples. Results correlate nearly perfectly with...

Formation of the hydrides of antimony arsenic, bismuth, germanium, lead, selenium, tellurium and tin by reaction with sodium tetrahydroborate0 affords an excellent method for the separation of these elements as gases from a wide range of matrices. Excellent low limits of detection are attained when this separation method is combined with atomisation of the hydride in a heated quartz tube in the...

Liquid chromatographs, coupled with graphite furnace atomic absorption spectrometers, have been widely used for the identification and quantification of trace element compounds. The quantification of the discontinuous signals from the spectrometer defining a chromatographic band is very much a matter of judgement and therefore prone to error. This paper describes a system which links a high-per...

Introduction: The therapeutic monitoring of lithium, through concentration measurements, is important for individual dose adjustment, as a marker of treatment adherence and to prevent poisoning and side effects. Objectives: Validate and compare two methods – atomic emission and atomic absorption – for the determination of lithium in serum samples. Methodology: Parameters such as specificity, pr...