A solid-phase extraction method for the preconcentration of Fe, Mn and Zn on a column containing Ambersorb 572 has been developed, and the determination of Fe, Mn and Zn in water using a flame atomic absorption spectrophotometer (FAAS) has been performed. The optimum preconcentration parameters of the procedure have been determined. The effect of the pH, complexing agent, amount of adsorbent, f...

Modification of a Perkin-Elmer 603 atomic absorption spectrophotometer by adding a high-intensity tungsten-halogen lamp for background correction significantly improved the detection limit for elements that have analytical wavelengths in the near-ultraviolet and visible regions. Chromium in human serum and urine can be measured, with a simplified sample-handling technique, in concentrations of ...

A method for total calcium in serum was optimized, a dual double-beam atomic absorption spectrophotometer being used, with strontium as an internal reference. The effect of HCI and lanthanum concentrations on the signals of both calcium and strontium was determined. The final analysis was unaffected by known sources of interference in serum at a 50-fold dilution of serum in 50mmolar HCI contain...

We describe an integrated, molecular-absorbance, atomic absorption instrument for studying metal/ligand binding in clinical samples. For an interface between the "high-performance" liquid chromatograph and the atomic absorption instrument we used a flow-injection sample manipulator, thus allowing both the chromatograph and the atomic absorption detector to operate at their separate optimum cond...

■ SPECTROPHOTOMETRY AND PHOTOMETRY Beer’s Law Spectrophotometric Instruments Components of a Spectrophotometer Spectrophotometer Quality Assurance Atomic Absorption Spectrophotometer Flame Photometry Fluorometry Chemiluminescence Turbidity and Nephelometry Laser Applications ■ ELECTROCHEMISTRY Galvanic and Electrolytic Cells Half-Cells Ion-Selective Electrodes pH Electrodes Gas-Sensing Electrod...