A simple, fast, and inexpensive voltammetric method for the simultaneous determination of trace bismuth(III) and lead(II) using (Hg(Ag)FE) as a working electrode was optimized. For adsorptive stripping voltammetric determination of Bi(III) and Pb(II) in a single scan, the cupferron was applied as a complexing agent. Experimental conditions under which these elements can be simultaneously detect...

Composites of bismuth and gold nanoparticles (Bi–AuNPs) were prepared on a carbon paste electrode (CPE) by an electrochemical deposition method. The electrochemical parameters were optimized for the effective deposition of Bi–AuNP composite materials. Microscopic examination revealed that nanoparticle clusters of gold were embedded well within the bismuth films (Bi films) over the surface of th...