Scanning transmission electron microscopy (STEM)-electron energy loss spectroscopy (EELS) has been used for studying local structure of the energy related materials. High resolution (Cs-corrected) STEM is regarded as a promising technique to observe morphological evolution and atomic arrangement inside single particles. Combining with EELS technique, one could probe the local chemical structure...

Two sets of hydrogenated microcrystalline silicon thin-film samples were prepared by Plasma Enhanced Chemical Vapor Deposition (PECVD) technique at different deposition conditions of excited power and pressure. The correlation between the crystalline volume fraction for the samples determined from Raman spectra and the excited power, pressure, absorption coefficient, refractive index and optica...

A pulsed metalorganic chemical vapor deposition (MOCVD) technique, specifically designed for high quality AlN/GaN superlattices (SLs) is introduced. Optical quality and precise controllability over layer thicknesses are investigated. Indium is shown to improve interface and surface quality. An AlN/GaN SL designed for intersubband transition at a telecommunication wavelength of ~1.5 μm, is grown...

TiO2 nanoparticles were synthesized by hydrothermal method at 180 ̊C from TiOSO4 aqueous solution with1m/l concentration. The obtained products were coated with silica by means of a seeded polymerization technique for a coating time of 1440 minutes to obtain well defined TiO2@SiO2 core-shell structure. The uncoated and coated nanoparticles were characterized by using X-Ray diffraction technique ...

Displacement of soil particles caused by erosion influences soil condition and fertility. To date, the cesium 137 isotope ((137)Cs) technique is most commonly used for soil particle tracing. However when large areas are considered, the expensive soil sampling and analysis present an obstacle. Infrared spectral measurements would provide a solution, however the small concentrations of the isotop...

An analytical technique to investigate the chemical state of trace metals in a small amount of sample has been proposed. While the principle for distinguishing the chemical state is based on well known X-ray spectroscopic phenomena, i.e., chemical shifts of the absorption edges, a total reflection mirror has been employed as a support to enhance the signal to background ratio through the reduct...

X-ray emission spectra recorded in the off-resonant regime carry information on the density of unoccupied states. It is known that by employing the Kramers-Heisenberg formalism, the high energy resolution off-resonant spectroscopy (HEROS) is equivalent to the x-ray absorption spectroscopy (XAS) technique and provides the same electronic state information. Moreover, in the present Letter we demo...

Abstract: A thermodynamic model was used to find out the optimum temperature for the growth of ZnS single crystals in closed ampoules by chemical vapor transport technique. Based on this model 1002 °C was found to be optimum temperature for 2 mg/cm3 concentration of transporting agent (iodine). ZnS Crystals were grown in optimum (1002 °C) and non-optimum (902 °C and 1102 °C) temperatures. The c...

We have proposed and experimentally demonstrated that picosecond time-resolved optical spectroscopy in the visible/near-infrared (NIR) region (700-1040 nm) is a useful technique for noninvasive characterization of wood. This technique has been demonstrated on both softwood and hardwood samples treated in different ways simulating the aging process suffered by waterlogged woods. In all the cases...

Atomic Absorption Spectrometry (AAS) is a technique for measuring quantities of chemical elements present in environmental samples by measuring the absorbed radiation by the chemical element of interest. This is done by reading the spectra produced when the sample is excited by radiation. The atoms absorb ultraviolet or visible light and make transitions to higher energy levels. Atomic absorpti...