نتایج جستجو برای: dispersive liquidliquid microextraction dllme

تعداد نتایج: 20479  

Journal: :iranian journal of pharmaceutical research 0
parvin parsaei department of chemistry, islamic azad university, north tehran branch, tehran, iran manouchehr bahmaei department of chemistry, islamic azad university, north tehran branch, tehran, iran. alireza ghannadi school of pharmacy and pharmaceutical sciences and isfahan pharmaceutical research center, isfahan university of medical sciences, isfahan, iran.

dispersive liquid-liquid microextraction method (dllme) combined with high-performance liquid chromatography-ultraviolet detection (hplc-uv) was used to determine thiamine (b1), nicotinamide (b3) and pyridoxine (b6) in sour cherry juice. this method was rapid, simple and sensitive. separation was accomplished using a c18 column. the optimum chromatographic conditions were found to be: mobile ph...

Journal: :Molecules 2014
Helena Prosen

Solvent extraction remains one of the fundamental sample preparation techniques in the analysis of environmental solid samples, but organic solvents are toxic and environmentally harmful, therefore one of the possible greening directions is its miniaturization. The present review covers the relevant research from the field of application of microextraction to the sample preparation of environme...

2016
AkbAR AkbARI

A new, rapid and highly sensitive and rapid method was proposed for the simultaneous determination trace levels of vitamin C and folic acid in the human urine samples. The inûuence affecting factors on the UA-DLLME such as type and volume of the dispersive and extraction solvent, pH, ionic strength and temperature of sample solution, sonication condition investigated and optimized. Under the op...

Journal: :Acta chimica Slovenica 2011
Mohammad Reza Hadjmohammadi Seyedeh Saboora Ghoreishi

A new method for the analysis of estrogens including estrone (E1), 17b- estradiol (E2) and diethylstilbestrol (DES) in aqueous samples was performed using dispersive liquid liquid microextraction (DLLME) and high- performance liquid chromatography (HPLC). In order to optimize DLLME some important parameters such as type and volume of extraction and disperser solvent, extraction time, ionic stre...

2013
Yaomei Hao Xuan Chen Shuang Hu Xiaohong Bai Deshuang Gu

Isomeric triterpenic acids of oleanolic acid (OA) and ursolic acid (UA) both have very low ultraviolet absorption and always exist in the same plant, so the separation and simultaneous determination of them have been a difficult task. In this study, a sensitive method combining dispersive liquid-liquid microextraction (DLLME) with HPLC-UV was developed for the extraction and determination of OA...

Journal: :Separations 2022

In the current study, an effective and simple procedure of extraction for four benzophenone compounds from water samples was achieved by dispersive liquid–liquid microextraction (DLLME) based on solidification floating organic droplets (SFO) with a natural monoterpene enol as extractant. As natural, high point, inexpensive, environmentally friendly hydrophobic solvent, α−terpineol selected firs...

Journal: :Turkish journal of analytical chemistry 2023

DLLME, which is a method that minimizes organic solvent consumption and waste generation, frequently used for trace analyte determination. In the present work, simple, selective sentsitive spectrophotometric based on dispersive liquid-liquid microextraction was reported. The procedure formation of 1:1 complex between Fe3+ water-soluble Cu(II) phthalocyanine then extraction this into dichloromet...

Journal: :Journal of analytical toxicology 2015
Manoj Kumar Gupta Rajeev Jain Pratibha Singh Ratnasekhar Ch Mohana Krishna Reddy Mudiam

Polycyclic aromatic hydrocarbons (PAHs) are ubiquitous environmental pollutants and well-known carcinogens. Hydroxy derivatives of PAH are considered as biomarkers of PAH exposure, and there is a need to measure these metabolites at low concentrations. So, a precise and eco-friendly analytical method has been developed for rapid determination of PAH metabolites. For the first time, a new analyt...

2015
Cátia M. Bolzan Sergiane S. Caldas Ednei G. Primel

Mineral water is known for its high purity. Because mineral water is produced by the infiltration of water through the soil, there is the possibility of contamination with pesticides. The aim of this study was to develop a simple, rapid and efficient method for the extraction and preconcentration of different classes of pesticides in mineral water samples by dispersive liquid-liquid microextrac...

Journal: :Journal of chromatographic science 2014
Xiaofang Liu Shu Zhou Quanfei Zhu Yong Ye Huaixia Chen

A sample pretreatment method, solid-phase extraction combined with dispersive liquid-liquid microextraction (SPE-DLLME), was established for the sensitive determination of polycyclic aromatic hydrocarbons (PAHs) in smoked bacon samples. In the SPE-DLLME process, three PAHs including naphthalene (Naph), phenanthrene (Phen) and pyrene (Pyr) were extracted from samples and transferred into C18 SPE...

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