Supercritical fluids extraction of emulsions (SEE) is an innovative technique used for the production of micro, nano-particles with controlled size and distribution. Supercritical carbon dioxide (SC-CO2) is used to extract selectively the organic solvents from the droplets of the emulsion, in which the biopolymer is dissolved, producing the precipitation of the polymer and the subsequent format...

High-quality N-doped graphene quantum sheets are successfully fabricated from as-grown monolayer graphene on Cu using nitrogen plasma, which can be transferred as a film-like layer or easily dispersed in an organic solvent for further optoelectronic or photoelectrochemical applications.

Dispersive liquid-liquid microextraction (DLLME) coupled with gas chromatography-flame ionization detection (GC-FID) was applied for the determination of two tricyclic antidepressant drugs (TCAs), amitriptyline and nortriptyline, from water samples. This method is a very simple and rapid method for the extraction and preconcentration of these drugs from environmental sample solutions. In this m...

Background: A syringe to syringe dispersive liquid phase micro-extraction-floating organic drop was applied and used for the simultaneous extraction and pre-concentration of trace amounts of amphetamine (AMP) and methamphetamine (MAMP) in urine samples. The extracted analytes were determined by high performance liquid chromatography along with diode array detection. Materials & Methods: In thi...

This work presented determination of some polycyclic aromatic hydrocarbons such as naphthalene, phenanthrene and acenaphthene in biological samples by Dispersive Liquid-Liguid Microextraction (DLLME) and gas chromatography. In this method, the appropriate mixture of extraction solvent (dichloromethane) and disperser solvent (acetone) are injected rapidly into the aqueous sample by syringe. Ther...

elevated atmospheric carbon dioxide and other green house gases have increased the earth temperature in recent century, which it affects all biochemistry cycles in soils. to examine the effect of atmospheric co2 concentration and temperature on n forms in soil solution in a calcareous soil, an experiment was conducted in a completely randomized design with factorial arrangement in the laborator...

novel dispersive liquid-liquid microextraction (dllme), coupled with high performance liquid chromatography with photodiode array detection (hplc-dad) has been applied for the extraction and determination of cyproheptadine (cph), an antihistamine, in human urine samples. in this method, 0.6 ml of acetonitrile (disperser solvent) containing 30 µl of carbon tetrachloride (extraction solvent) was ...

Within international research in partitioning and transmutation (P&T), the separation of trivalent actinides (An(III)) from the chemical similar trivalent lanthanides (Ln(III)) is a main task that was comprehensively studied within the last two decades [1–3]. The investigated solvent extraction processes often follow the plutonium uranium reduction extraction (PUREX) process, in which uranium a...

The present study was carried out between September 2019 and March 2020 in Yıldız River, which is located within the borders of Yıldızeli district Sivas province used for agricultural irrigation purposes, to determine chemical characteristics river water trace elements. Water’s alkalinity, oxygen demand (COD), chloride (Cl-), calcium (Ca2+), total hardness, phosphate (PO4-P), dissolved reactive...

A simple and rapid vortex assisted ionic liquid based liquid-liquid microextraction technique (VALLME) was proposed for preconcentration of trace levels of cadmium. According to this method, the extraction solvent was dispersed into the aqueous samples by the assistance of vortex agitator. Cadmium preconcentration was mediated by chelation with the 8-hydroxyquinoline (oxine) reagent and an IL, ...