Polyimide/Nickel oxide (polyimide/NiO) nanocomposite was successfully synthesized by sol gel technique, using Pyromellitic dianhydriede (PMDA), 4,4-oxydianiline (ODA) and N,N-dimethylacetamide (DMAC) and 10 wt% Nickel titanate nanopowders (NPs). Fourier transform infrared spectrometry (FTIR), X-ray diffraction (XRD), scanning electron microscopy (SEM), and vibrating sample magnetometer (VSM) we...

Polyimide/Nickel oxide (polyimide/NiO) nanocomposite was successfully synthesized by sol gel technique, using Pyromellitic dianhydriede (PMDA), 4,4-oxydianiline (ODA) and N,N-dimethylacetamide (DMAC) and 10 wt% Nickel titanate nanopowders (NPs). Fourier transform infrared spectrometry (FTIR), X-ray diffraction (XRD), scanning electron microscopy (SEM), and vibrating sample magnetometer (VSM) we...

Wetting of the pore walls of porous templates is a simple and convenient method to prepare nanotubes. Ferroelectric lead zirconate titanate and barium titanate nanotubes were fabricated by wetting of porous silicon templates of polymeric precursors. The ferroand piezoelectric properties of an individual ferroelectric either of a PZT or a BaTiO3 nanotube were electrically characterized by measur...

Magnetoelectric (ME) composites that simultaneously exhibit ferroelectricity and ferromagnetism have recently gained significant attention as evident by the increasing number of publications. These research activities are direct results of the fact that multiferroic magnetoelectrics offer significant technological promise for multiple devices. Appropriate choice of phases with co-firing capabil...

Doped piezoceramic lead zircanate titanate has been characterized in the frequency range of 20–60 MHz using ultrasonic spectroscopy. Theoretical analyses were performed for the reflection and refraction of acoustic waves at the interface of water-piezoelectric ceramic. The incident directions of the wave were chosen to be appropriate for ultrasonic spectroscopy measurements. Shear wave spectrum...

This work describes the application of two different test structures to execute broadband microwave measurements of the dielectric constant of ceramic thin films. Coplanar waveguide probes and vector network analyzer were used to measure the dielectric constant versus frequency of thin films of lead zirconate titanate and zirconium titanate, fabricated by sol gel methods. One-step lithography w...

Ž . Ultrafine lead titanate PbTiO powders in tetragonal form have been successfully prepared via two processing routes, 3 Ž . Ž . namely, conventional coprecipitation CPC and microemulsion-refined coprecipitation MCP . The formation process of lead titanate from the resulting precursors was monitored using techniques such as thermal analyses, FTIR spectroscopy, Raman scattering spectroscopy and...

The photochemical growth of silver nanoparticles on the negative domains of lead zirconate titanate thin films is reported. A sample of highly [100] orientated lead zirconate titanate, with a ratio of 30:70, that was 65-70 nm thick grown on Pt-coated MgO was poled by use of piezoresponse force microscopy to produce defined regions of surface positive and negative polarization. A comparison betw...

A new concept for preparing hollow metal oxide nanopowders by salt-assisted spray pyrolysis applying nanoscale Kirkendall diffusion is introduced. The composite powders of metal oxide and indecomposable metal salt are prepared by spray pyrolysis. Post-treatment under a reducing atmosphere and subsequent washing using distilled water produce aggregation-free metal nanopowders. The metal nanopowd...