nanocomposite of zro2/zno was prepared under ultrasonic irradiation by sol gel process from directly mixing zirconium and zinc gels, and the mixture was placed under ultrasonic irradiation for 2 hours then aging time the filtrated composite gel was calcinated at 500°c for 3h in furnace. the precursor sol of zirconium was prepared from an aqueous solution of zrcl4 and zinc acetate dihydrated was...

PURPOSE The purpose of this in vitro study is to examine the effects of a nano-structured alumina coating on the adhesion between resin cements and zirconia ceramics using a four-point bending test. MATERIALS AND METHODS 100 pairs of zirconium bar specimens were prepared with dimensions of 25 mm × 2 mm × 5 mm and cementation surfaces of 5 mm × 2 mm. The samples were divided into 5 groups of 2...

pure anatase titania (tio2), mixed 1.0 wt.% cerium-anatase titania (1.0 wt.%ceo2-tio2), and mixed 1.0 wt.% zirconia-anatase titania (1.0 wt.%zro2-tio2) nano powders were synthesized by co-precipitation method and characterized using x-ray diffraction (xrd), brunauer-emmett-teller (bet) surface area analysis, uv-vis diffuse reflectance spectroscopy (drs), and transmission electron microscope (te...

an efficient and green protocol for the synthesis of pyrazoles derivatives by one-pot reaction of different 1,3-dicarbonyl compounds with hydrazines/hydrazides has been developed using nano-sulfated zirconia, nano-structured zno, nano-g-alumina and nano-zsm-5 zeolites, as the catalyst. the optical properties of the nano-structured catalysts and organic molecules were studied. the advantages of ...

PURPOSE The purpose of this study was to evaluate the effect of nano-structured alumina surface coating on shear bond strength between Y-TZP ceramic and various dual-cured resin cements. MATERIALS AND METHODS A total of 90 disk-shaped zirconia specimens (HASS CO., Gangneung, Korea) were divided into three groups by surface treatment method: (1) airborne particle abrasion, (2) tribochemicalsil...

The ballistic impact performance of nanocrystalline zirconia-toughened alumina (nZTA) ceramics, comprising 15 wt% nano-yttria-stabilised zirconia in a sub-micron matrix, have been studied through depth penetration tests and compared to the results for monolithic alumina. resistance each material was evaluated by fitting against thickness ceramic targets. These show that, despite micro-Raman ana...

The phases of ceria–zirconia nanoparticles observed in air are studied as a function of particle size and composition by X-ray diffraction, transmission electron microscopy, and Raman spectroscopy. The emergence of two tetragonal phases t00 and t monotonically moves toward higher zirconia concentrations with decreasing particle size. A smaller particle size increases the solubility of zirconia ...

Spray drying is widely used for producing granulated feed materials for compaction process, which is the current industrial method for manufacturing alumina-zirconia femoral heads. The optimization of the granules compaction behavior requires the control of the slurry rheology. Moreover, for a dual-phase ceramic suspension, the even phase distribution has to be kept through the atomization step...