نتایج جستجو برای: parahydrogen

تعداد نتایج: 287  

2015
Milton L. Truong Thomas Theis Aaron M. Coffey Roman V. Shchepin Kevin W. Waddell Fan Shi Boyd M. Goodson Warren S. Warren Eduard Y. Chekmenev

NMR signal amplification by reversible exchange (SABRE) is a NMR hyperpolarization technique that enables nuclear spin polarization enhancement of molecules via concurrent chemical exchange of a target substrate and parahydrogen (the source of spin order) on an iridium catalyst. Recently, we demonstrated that conducting SABRE in microtesla fields provided by a magnetic shield enables up to 10% ...

Journal: :Physical chemistry chemical physics : PCCP 2012
Rolando R Lozada-García Justinas Ceponkus Michèle Chevalier Wutharath Chin Jean-Michel Mestdagh Claudine Crépin

The photochemistry of the chelated enol form of acetylacetone (AcAc) was investigated by UV excitation of the S(2) state at 266 nm in parahydrogen matrices, complemented by experiments in neon and normal hydrogen matrices. Infrared (IR) spectroscopy, combined with theoretical calculations, was used to identify the photoproducts. Isomerization towards various non-chelated forms (no intramolecula...

Journal: :Chemical Communications 2018

Journal: :Angewandte Chemie International Edition 2020

2013
Haifeng Zeng Jiadi Xu Joseph Gillen Michael T. McMahon Dmitri Artemov Jean-Max Tyburn Joost A.B. Lohman Ryan E. Mewis Kevin D. Atkinson Gary G.R. Green Simon B. Duckett Peter C.M. van Zijl

Hyperpolarization produces nuclear spin polarization that is several orders of magnitude larger than that achieved at thermal equilibrium thus providing extraordinary contrast and sensitivity. As a parahydrogen induced polarization (PHIP) technique that does not require chemical modification of the substrate to polarize, Signal Amplification by Reversible Exchange (SABRE) has attracted a lot of...

Journal: :Physical review letters 2004
M S Anwar D Blazina H A Carteret S B Duckett T K Halstead J A Jones C M Kozak R J K Taylor

Here we demonstrate how parahydrogen can be used to prepare a two-spin system in an almost pure state which is suitable for implementing nuclear magnetic resonance quantum computation. A 12 ns laser pulse is used to initiate a chemical reaction involving pure parahydrogen (the nuclear spin singlet of H2). The product, formed on the micros time scale, contains a hydrogen-derived two-spin system ...

2008
M. Roth J. Bargon H. W. Spiess A. Koch

Introduction Parahydrogen induced polarization (PHIP) has turned out to be a versatile technique to obtain hyperpolarized molecules exhibiting strong NMR signals via a chemical approach. PHIP makes use of breaking the high initial symmetry of parahydrogen during homogeneously catalyzed hydrogenations of unsaturated substrates and, therefore, of the creation of nonequivalent protons in the produ...

Journal: :Journal of Chemical Physics 2021

The diffusion and reactivity of hydrogen atoms in solid parahydrogen at temperatures between 1.5 K 4.3 are investigated by high-resolution infrared spectroscopy. Hydrogen produced within as the by-products 193 nm situ photolysis N2O, which induces a two-step tunneling reaction, H + N2O ? cis-HNNO trans-HNNO. second-order rate constant for first step to form is found be inversely proportional co...

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