A multi-residue method based on modified QuEChERS sample preparation with multi-walled carbon nanotubes (MWCNTs) as reversed-dispersive solid phase extraction (r-DSPE) material and gas chromatography-mass spectrometry determination by selected ion monitoring (GC/MS-SIM) mode was validated on 30 representative pesticides residues in vegetables and fruits. The acetonitrile-based QuEChERS (quick, ...

This application note describes a simple and rapid extraction procedure for pesticide residues in lemon essential oils. The method uses Agilent Bond Elut QuEChERS extraction and modified dispersive SPE coupled with GC/MS. Author Limian Zhao and Joan Stevens Agilent Technologies, Inc. 2850 Centerville Road Wilmington, DE 19808 USA Application Note

a fast and simple modified quechers (quick, easy, cheap, rugged and safe) extraction method based on spiked calibration curves and direct sample introduction was developed for determination of benzo[a]pyrene (bap) in bread by gas chromatography-mass spectrometry single quadrupole selected ion monitoring (gc/ms-sq-sim). sample preparation includes extraction of bap into acetone followed by clean...

QuEChERS (quick, easy, cheap, effective, rugged, and safe) sample preparation methods have been developed to help monitor pesticides in a range of food samples. These methods require many manual steps, such as shaking, centrifugation, and dispersive SPE cleanup, making it a quite labor-intensive process. There is a need for automating parts of QuEChERS extraction in order to improve laboratory ...

Citation: Guerreiro TM, Ozawa KS, Lima EdO, Melo CFOR, de Oliveira DN, Triano SPdN and Catharino RR (2018) New Approach of QuEChERS and GC-MS Triple-Quadrupole for the Determination of Ethyl Carbamate Content in Brazilian cachaças. Front. Nutr. 5:21. doi: 10.3389/fnut.2018.00021 new approach of Quechers and gc-Ms Triple-Quadrupole for the Determination of ethyl carbamate content in Brazilian ca...

A comprehensive review is presented on the recent developments and trends in the QuEChERS (quick, easy, cheap, effective, rugged, and safe) sample preparation approach. This technique involves liquidliquid partitioning using acetonitrile and purifying the extract using dispersive solid-phase extraction (d-SPE). Originally, the QuEChERS was introduced for pesticides residues analysis in high moi...

This application note describes a simple and rapid extraction procedure for pesticide residues in lemon essential oils. The method uses QuEChERS extraction and modified dispersive SPE coupled with GC/MS. Author Limian Zhao and Joan Stevens Agilent Technologies, Inc. 2850 Centerville Road Wilmington, DE 19808 USA Application Note

A simple and high-throughput screening method for the analysis of 136 pesticides in avocado ( Persea americana ) by LC-(+)-ESI-MS/MS and GC-MS/MS is presented. A modified QuEChERS sample preparation method was developed to improve the extraction recovery of highly lipophilic pesticides. Extracts from minced avocados after acetonitrile (MeCN) extraction were directly injected to LC-MS/MS, wherea...