Europium-doped yttrium silicate (Y2SiO5:Eu ) nanophosphors were successfully synthesized by flame spray pyrolysis method. The effect of silicon concentration on the crystal structure and morphology of the Y2SiO5:Eu 3+ phosphors were investigated. Asprepared phosphor consists of spherical nanoparticles with filled morphology, high crystallinity, narrow size distribution, and intense photolumines...

Flame Spray Pyrolysis (FSP) is a well investigated high temperature aerosol technique for synthesizing nano-sized metal oxide catalysts of almost all metals and transition metals by gas-to-particle conversion (Teoh et al. 2010). However, specific designs of multi-component catalysts and the controlled dispersion of catalytic material on the support are limited with this approach. Double Flame S...

A mullite/mullite nanocomposite powder has been synthesized, composed of nanometer-size 3Al2O3 · 2SiO2 (‘3 : 2’) mullite precipitates within a matrix of the high alumina 2Al2O3 · SiO2 (‘2 : 1’) mullite. Historically, the transition from the metastable high-alumina phase to the thermodynamically stable ‘3 : 2’ phase of mullite has been thought to be a continuous process, involving a continuous s...

The hydrodesulfurization (HDS) activity of molybdenum sulfide-based catalysts is localized to the edges of this layered solid and is, therefore, highly dependent on the technique used to prepare the material. Here, ultrasonic spray pyrolysis (USP) was used to synthesize porous, nanostructured MoS2. Low surface area powders, not useful for catalysis, are generally produced by USP. This work show...

Photoluminescence of highly structured ZnO layers comprising well-shaped hexagonal rods is presented. The ZnO rods (length 500-1,000 nm, diameter 100-300 nm) were grown in air onto a preheated soda-lime glass (SGL) or ITO/SGL substrate by low-cost chemical spray pyrolysis method using zinc chloride precursor solutions and growth temperatures in the range of 450-550°C. We report the effect of th...

Porous carbon spheres with unique structures and morphologies are prepared from energetic carbon precursors, alkali propiolates, via ultrasonic spray pyrolysis. Aerosolized liquid droplets containing alkali propiolates act as microreactors that confine the thermal decomposition of energetic precursors and lead to the formation of several unprecedented carbon morphologies.

Carbon-iron oxide microspheres' black pigments (CIOMBs) had been prepared via ultrasonic spray pyrolysis of aqueous solutions containing ferrous chloride and glucose. Due to the presence of carbon, CIOMBs not only exhibited remarkably acid resistance, but also could be well dispersed in both polar solvents and nonpolar solvent. Finally, dispersions of hollow CIOMBs in tetrachloroethylene had su...

An indigenously developed chemical spray pyrolysis system was used to deposit polycrystalline CuInS2 thin films. It was found that smaller spray rate results in films with better crystallinity and lower resistivity. Increase in surface roughness of the films was observed for higher spray rates. Variations in film stoichiometry with composition of spray solution were analyzed along with its opto...

Pure and mixed ZnO-SiO2 particles were prepared by flame spray pyrolysis (FSP) of zinc acetate (ZA) and either hexamethyldisiloxane (HMDSO) or SiO2-sol dispersed in either methanol or a water-in-oil emulsion. The product particles were characterized by nitrogen adsorption, infrared absorption and X-ray diffraction. The evolution of solid or hollow particle formation along the flame axis was elu...