In this paper, synthesised nanometre sized hydroxyapatite (nano-HAP) powders composed of spherical 30 ± 5 nm part icles were compacted and sintered at temperatures ranging from 650 to 1250°C to form ceramics of varying porosity and mechanical strength. The size, crystalline structure and morphology of both the synthesised nano-HAP particle powders and the compacted and sintered ceramics were in...

An electric-current-assisted method was used to mineralize dense hydrogels and create hydroxyapatite/hydrogel composites with unique hierarchical structures. The microstructure of the final material can be controlled by the mineralization technique and the chemistry of the organic matrix. A hydroxyapatite/hydrogel composite was obtained with a large inorganic content (approximately 60% of the w...

The effect of extrinsic porosity on the reduction behavior FeO was evaluated by thermogravimetric analysis (TGA), scanning electron microscopy (SEM) and Brunauer–Emmett–Teller (BET) technique analyzed using labyrinth coefficient FeO. pore exhibited an abnormal in range less than 50% degree, despite increase apparent porosity. SEM BET indicated that pores at initial stage speculated to be due ch...

Nickel molybdate (NiMoO₄) nanoparticles were synthesized via calcination of an oxalate complex in static air at 500 °C. The oxalate complex was analyzed by thermal gravimetric analysis (TGA) and Fourier transform infrared spectroscopy (FTIR). The as-synthesized nickel molybdate was characterized by Brunauer-Emmett-Teller technique (BET), X-ray diffraction (XRD), and transmission electron micros...

Ordered nanoporous silicas containing various binary copper-manganese oxides were prepared as catalytic systems for effective carbon monoxide elimination. The carbon monoxide elimination efficiency was demonstrated as a function of the [Mn]/[Cu] ratio and reaction time. The prepared catalysts were characterized by Brunauer-Emmett-Teller (BET) method, small- and wide-angle X-ray diffraction (XRD...

Benzene is one of the target compounds to be removed from air owing to its carcinogenicity. In this study, benzene oxidation with ozone over a MnOx/KIT-6 catalyst was carried out for the first time. MnOx/KIT-6 was synthesized using two different Mn precursors: Mn acetate and Mn nitrate. The characteristics of the synthesized catalysts were examined by X-ray diffraction, X-ray photoelectron spec...

in the present study, different activated carbons were prepared from carbonized african beech wood sawdust by potassium hydroxide activation. the activated carbons were characterized by brunauer–emmett–teller, scanning electron microscope, fourier transform infrared spectroscopy, and thermogravimetric analyzer. the phenol adsorption capacity of the prepared carbons was evaluated. the different ...

We have synthesized, characterized, and computationally simulated/validated the behavior of two new metal-organic framework (MOF) materials displaying the highest experimental Brunauer-Emmett-Teller (BET) surface areas of any porous materials reported to date (~7000 m(2)/g). Key to evacuating the initially solvent-filled materials without pore collapse, and thereby accessing the ultrahigh areas...

In this work, Cs ion sorption on some clays and zeolite were investigated. Cs was used as a tracer. Activities were measured with a NaI crystal gamma counter. The particle size distribution was determined by a laser sizer. Surface area of the particles were determined by BET (Brunauer, Emmett and Teller method). Structure analysis was made by using X-ray diffraction. The chemical compositions o...

the silica aerogel was prepared by the acid–base sol–gel polymerization of tetraethylorthosilicate precursor followed by ambient pressure drying. the prepared silica aerogels were characterized by fourier transform infrared )ft-ir(, thermo-gravimetric and differential thermal analysis )tg/dta(, x-ray diffractometer )xrd(, energy dispersive x-ray microanalysis )edx(, brunauer–emmitt–teller (bet)...